Uneven slumps

Credit: Lara Duncan

Uneven slumps – where the glass does not slide down the sides evenly, leaving one side higher than the other – are common in moulds with steep sides.  Another common cause is uneven weight on the blank – where there are more layers on one side than another.  Yet another common cause of uneven slumping is the blank having large areas of glass with different viscosities.

Things I can think of to avoid the problem.

While the glass is firing

Use a moderate rate of advance to the target temperature. Once that is reached, peek every 10 minutes to observe how the slump is proceeding.  When the slump begins to go off centre, reach in with protective gear and adjust it back to even.  The kind of protective gear you need is shown in this post.

An alternative to moving the glass is to tip the mould.  If the mould is relatively shallow with a flat bottom,  there is not much you can achieve by this action.  On deeper moulds, you can elevate one side of the mould.  This puts the elevated side closer to the top and so into a hotter part of the kiln.  This means that you elevate the side that is not slumping as quickly.  You do this because the slowly slumping glass needs more heat in relation to the faster slumping side.  It seems counter intuitive, until you realise you are putting the slow side into greater heat.  You will need to continue observing at intervals to know when the glass is slumping evenly. At that point you can return it to level.

I admit that moving the glass is my choice almost all the time.  It works well on moderately deep moulds.  Elevating one side of the mould while firing requires more time in the kiln that I want to give.  Tipping the mould works best on very deep moulds and so I view it as a special case.

Before the slumping begins

Most of the time we make our blanks the same diameter/dimension or slightly larger than the mould. This allows the glass to rest on the rim and be certain it is as level as the rim of the mould is.  However, this also creates an edge which the glass needs to slide over as it slumps.  Especially with steep sided moulds.

A fix for this is to make the blank fit just inside the rim.  Then it does not have to slide over the rim, and avoids the risk of hanging up on one part rather than another.  You will need to ensure the glass is level within the mould as well as the mould itself, in this case.  If you take this approach of internal placing and you want a piece with a particular final dimension, you should buy a mould larger than the final size needed.

You can combine this placing of the glass internally with another preventative for uneven slumps in deep moulds.  You can grind a small bevel on the underside of the edge to help the glass have greater contact with the mould, so resisting uneven movement.  This can be done separately from fitting the glass inside a steep sided mould, but is most likely to be successful if performed on a blank smaller than the mould dimensions.

Uneven slumps in kilnforming can be corrected during the firing or by preparation of the blank in relation to the mould before the firing.

Further information is available in the ebook: Low Temperature Kiln Forming.

Calibrating your new kiln

My new kiln fires differently than my existing one(s).

Each kiln will be different in minor or major ways.  Suggested schedules are only starting points, even though they worked in your previous kiln. You need to learn about your new kiln’s characteristics in the same way you did with your first kiln. There are a number of ways to do this.

Many people recommend making test tiles for the different levels of fusing that you use and at different temperatures to determine which is the best for your new kiln.  Additionally, you need to note the rate(s) at which you fired these samples to make the test tiles accurate representations of firings.  Yes, these will be good references.  And yes, they are valuable if you have the time for all these firings.

 Idle Creativity

Observation during the firing of test tiles is the best and quickest way to discover how your new kiln is performing at various temperatures.  In one firing you can note the temperatures at which the various tack levels occur, and the contour and full fuse temperatures.  You can even take pictures through the peep hole of your kiln (as long as you don’t put the camera too close to the kiln!).  This procedure will make knowing your kiln much quicker and accurate than unobserved multiple firings.

To make use of the notes of the temperatures where the results were achieved in the test firing, back off 10°C (or 20°F) from the observed temperature and add 10 minutes processing time.  You may find after a few uses of these temperatures you may want to adjust the temperature a bit more, but you will have done the major experimental work in one firing.

It is a good idea to set up other test tiles and run the experiment again at a slower rate of advance.  This will give you information about how the different rates of advance affect the processing temperature and the look and texture of the piece, especially on the bottom.  The texture imparted at different processing temperatures becomes more important in slumping and draping processes.

In another firing you can set up various moulds and observe when the slumps or drapes are complete. Recording this information lets you know slump temperatures for various styles and spans of moulds.  Make sure you record the temperatures that the pieces slump fully into the mould. You can then back off 20°C from those points and add 30 minutes as a starting point for you actual slumping firings.

New kilns require experience to know what the appropriate temperatures are.  Buy setting up test tiles you can observe in one firing the various levels of fuse from tack to full fuse, so saving lots of firing time.

Further information is available in the ebook: Low Temperature Kiln Forming.

Single Layer Circle with Decorative Rim

A question arose:

If you fuse a single 20cm diameter sheet of 3mm glass to full fuse, [with a decorative rim] what happens? … Would the lack of two layers in the centre be a problem for the 6mm rule?

This layup risks trapped air and a large central bubble.  The explanation involves the combination of volume control and weight.

Volume control

The volume control relates to the single 3mm layer in the centre.  The glass will thin in the centre and thicken at the perimeter.  This leads to the risk of thinning to the degree that bubbles are created in the centre.  The edges will also draw in as the viscosity - surface tension - of the glass pulls the glass toward a 6mm thickness.

Weight

The explanation is also about weight.  The decorative rim adds weight to the outside of the piece.  This weight will “seal” the rim of the glass to the shelf, reducing the possibility of air escaping from under the central portion of the piece.  This weight effect on the rim increases the risk of a large central bubble.

Profile

Another influence on the result of the fuse is the degree of fuse.  At full fuse the viscosity of the glass is less and so resists the force of expanding air much less than when cooler. Even at rounded tack fuse, the glass will be unable to resist the formation of bubbles. As the glass thins and viscosity decreases, any air at all will cause a bubble.

Changes for the future

Avoidance of bubbles in this piece relate to design, scheduling and technique.

Design

It is possible to design a piece of this nature to avoid the volume control issue.  The base piece could have a smaller circle or rectangle centralised on top inside the proposed perimeter.  The rim can then have the decorative elements placed.  If they are spaced widely, frit can be used to fill significant gaps.  The piece can then be placed in the kiln for a full fuse.

Scheduling

You can also fire the piece as originally described very slowly to a low temperature.  This uses the concept of heat work. By applying the heat over a long period, you can achieve the same effect as would be achieved by a faster rate of advance to a higher temperature. 

There are at least two ways to increase the heat work.  You can use a very slow rate of advance to a point slightly above the softening point of the glass.  This will be the lower end of the slumping temperature range of your glass.  The soak may be for hours.  You will need to observe when the effect you want is achieved.

You also can choose the same lower slumping temperature and reach it in your standard fashion.  This will require an even longer soak time to achieve the same result.

In both these low firing approaches, you will need to observe to determine when the piece is finished.

Technique

The “flip and fire” technique may also work on the single layer with an added rim.  To do this you build the piece upside down on the shelf.  It helps to draw an outline of design on Thinfire, or Papyros.  Place the decorative elements and cap them with the clear.  Take the whole to a rounded tack fuse.  When cool, clean well and fire to a tack fuse again.  This will give something less than a full fuse, but it will be more than a tack, as the heat work is cumulative.

Further information is available in the ebook Low Temperature Kiln Forming.

Summary

A single layer piece with a decorative rim is most likely to produce bubbles in the centre.  There are some ways to overcome this: design, scheduling, and technique. Design is the most likely to be successful.

Texture Moulds and Glass Sizes

I had an overhang [on a texture mould] and I heard a pop and opened kiln and saw it cracked off the mold. … [The piece] is 2 layers Bullseye irid placed face down and Tekta [on top]; the mold was sprayed 3-4 times with zyp and Thinfire; and I put mold on kiln posts. [I] fired to 1440[F].

Diagnosis 

The overhang of the glass caused the break. As the glass heats it expands. The ceramic does not expand as much as the glass.  This means even more glass will hang over the edge than at the start.  As the glass reaches slumping temperatures, it begins to drape over the edge. At the same time the glass on the interior is beginning to slump into the textures.  When the glass has fully taken up the texture, the overhanging glass will be touching the outer sides of the mould. This means at the end of the heating and soaking part of the firing, you have the ceramic mould partially and tightly encased in glass.  The glass has formed around the ceramic.

Credit: theavenuestainedglass.com

The physics of the two materials are that glass expands more than ceramic. On cooling, the glass grips the sides of the ceramic mould tightly. This is because it shrinks more than the ceramic.  In this case, the ceramic was stronger than the glass and the strain caused the glass to break.  Upon occasion the opposite can happen.

Two other notes.

The temperature of 781°C is higher than needed.  You will need to do a bit of experimentation to find the right combination of temperature and time for each mould.  You could consider 630°C as an initial temperature with a 90-minute soak.  Bob Leatherbarrow (p.161) describes a method of scheduling a sequence of slightly higher temperatures with soaks.  If the texture is not forming (as determined by observations), you can advance to the next segment with a higher temperature and see how that goes.  When the appropriate amount of texture has been achieved, advance to the cooling to anneal segment.

Iridised surfaces provide a very good separator.  With the iridisation down against the mould, it may be unnecessary to use Thinfire, especially when you already have used boron nitride as the separator.

Further information is available in the ebook: Low Temperature Kiln Forming.

Incomplete definition on texture moulds

An enquiry on incomplete definition in the glass from texture moulds:

I have this texture mould, but I’m not getting much definition. I’m using a single 3mm layer of 96. Do I need to go hotter for longer?

155C - 750C, 15 minutes

Full - 516C, 140 minutes

49C - 371C, 0 minutes

Full - 49C, off

My response:

You have sensibly increased the temperature at a moderately slow rate (for 3mm).  This ensures the glass is evenly heated through by the time it reaches the working temperature.  It is slow enough for you to be confident that most of the air has been squeezed out.

If you wanted to be more cautious about bubbles,  you could introduce a slow increase in temperature - maybe 50°C - from 600°C to 650°C.  You may want to soak there for 30 minutes, although it may not be necessary.  Once that segment is finished you can resume at 75°C to the top temperature.

I would not increase the temperature as you are already at risk of dog-boning the glass.  I would extend the soak time to 180 minutes at 750°C. You need to check frequently after the top temperature is achieved.  A quick peek is all that is required to see if the texture is fully reflected in the top surface.  You may find success by using a lower temperature, say 730°C, but it will require at least an hour more soak time.

The piece above conformed completely to the 12mm depth of the mould with a soak of three hours at 750°C. There was incomplete formation of another test piece at 740°C for three hours. So the 10°C made enough difference for complete formation over this depth.  With less extreme heights, a lower temperature or a shorter soak would be possible.

Once the texture is assured, you need to advance to the next segment.  Or, if it is not achieved by 10 minutes before the end, extend the soak.  Check your controller manual on how to skip to the next segment, or to extend the soak.

As an aside, your annealing soak and cool is very long and slow for 3mm.  You can regain the time used in the slow ramp rate and soak. Review the requirements for a single sheet of glass.  A 60-minute annealing soak and a cool rate of 83°C/hr. to 370°C is an adequately slow anneal cool for a 3mm piece.

You may find more success with a 6mm sheet.  The weight of glass helps it conform to the texture mould.  I have found that a slow ramp rate (about 150°C) to the strain point of ca. 540°C, followed by half that rate to top temperature allows a reduction in soak time to achieve the required definition. This reduction in soak time can be one half hour less than the time required to get good definition on a 3mm sheet.

The strategy outlined here for the scheduling is using the principle of slow and low and long firings.  It is much easier to control the results of the firing by using moderate ramp rates to lower temperatures combined with longer soaks and periodic peeking to check on progress.

If you do not have the time to devote to peeking when the schedule is at the top temperature, you should investigate the method of programming a delay to the start of the firing.  Your controller manual will give the method of using this function.

Texture moulds work well with the slow and low principle of kilnforming.  Long soaks may be required with periodic observation to determine when the process is complete.

Further information is available in the e-book: Low Temperature Kilnforming.

Texture moulds

"I could use some help here please. I’ve tried this sun mould 3x and as you can see all 3x I get a hole.  If you could tell me what I’ve done wrong I would greatly appreciate. They were all full fused to 1430F (776C)."

Example of the problem

There are a range of views that have been given on how to make texture moulds work without the glass developing bubbles.

closer view of one example

These are a summary of the suggestions made to the enquirer.

Not enough glass thickness. The view is that glass needs to be 6mm thick to be used on texture moulds, as the viscosity of glass tends to draw glass to that thickness, robbing from other areas making them thin and prone to bubbles.

Glass always wants to go to 6mm.  Not always.  It depends on temperature.  The kiln forming temperatures we use results in a viscosity that tends to equalise the forces at 6 – 7 mm.  Hotter glass will flow out more thinly, until at about 1200C, the glass is 1mm or less thick.

Full fuse two sheets first.  The object is to avoid placing two separate sheets on top of the mould, creating the potential for more bubbles between the sheets, as they may slump into the mould at different rates.

Too hot. As the glass increases in temperature the viscosity is reduced and can no longer resist the air pressure underneath the glass.

Use a lower temperature. The idea is to keep the glass relatively stiff to resist bubble formation.

Bubble squeeze needed to avoid trapped air.  Another way to reduce the amount of air under the glass is to allow the glass to relax slowly at a temperature below which the glass becomes sticky.

Elevate the mould.  The idea is that hot air circulating under the mould will help equalise the temperature of the mould and the glass.

Drill holes at low points. This gives air escape routes under the mould, assuming the mould is slightly elevated.

Go lower and slower.  Use a slower rate of advance toward a lower top temperature with longer soaks to avoid reducing the viscosity, but still get the impression from the mould.

Now for a different viewpoint.

None of the views given above are wrong, but they all (except in one case) fail to consider the fundamentals of obtaining texture from such a mould.

It is apparent that the temperature used was too high because the glass had low enough viscosity to allow the air underneath to blow the bubble.  The suggestions of thicker glass, bubble squeezes, lower temperatures, drilling holes and elevation of the mould are ways of reducing the amount of air or resisting the air pressure.  They are not wrong, but miss the fundamental point.

That fundamental point is that you need to raise the temperature slowly on these texture moulds to allow the glass to fully heat throughout. By doing this most of the air has a chance to filter out from under the glass before it conforms to the edges of the mould.  It is simpler to use the slow advance rather than a quick one with a slow-down for a bubble squeeze.  The glass is more certain to be the same temperature throughout by using a slow rate of advance.  Glass with an even temperature can conform more easily to the undulations and textures of the mould.

Mostly, the recommendations given are to use two layers, or 6mm of glass that has already been fused together.  This gives greater resistance to bubble formation and reduces the dogboning and needling of the edges.

However, you can form in these moulds with single layers.  There are of course certain conditions:

• You must advance the temperature slowly.  A rate of 100C per hour will be fast enough.
• You can add a bubble squeeze soak of 30 minutes at about 630C as additional assurance of removing most of the air.  The bubble squeeze is done at a lower temperature than usual, as the glass is less viscous because the slow rate of advance has put more heat work into the glass.
• The top temperature should not go beyond 720C. Beyond that temperature the viscosity of the glass drops quickly and so becomes subject to bubble formation.

The soak at the forming temperature will need to be long and observation will be needed to determine when the glass has fully conformed to the mould. Quick peeks at intervals will show when the design is visible on the top of the glass. The time will vary by:

• Mould texture complexity 
• Type of glass (opalescent or transparent),
• Heat forming characteristics of the glass,
• Viscosity of the glass or colour,
• Etc. 

Be knowledgeable about how to extend the soak or to advance to the next segment of the schedule to take advantage of your observations.

Your observation may show that you can do the texture formation at a lower temperature in future. This will provide results with less separator pickup and better conformation to the mould without excessive marking. 

You will need a long soak in either circumstance. This will be in terms of hours not minutes.  If you do these texture moulds at slumping temperatures, you will probably need at least twice your normal soak.

You can do a lot to fool the single layer glass into doing what you want by using low temperatures and long soaks. See Bob Leatherbarrows's book on Firing Schedules.  He gives a lot of information on how to manipulate glass through heat work - the combination of temperature and time.  You might also consider obtaining my book - Low Temperature Kilnforming.

Most of the search for the right temperature, fails to note that the important element is how you get to the temperature. You can get the same result at different temperatures by using different rates of advance.

Kilnforming is more than temperature, it is also about time and the rate of getting to the temperature. By concentrating on temperature, we miss out on controlling the speed and the soak times. You can do so much more to control the behaviour of the glass at slow rates, significantly long soaks, and low temperatures.

Convex Shapes for Wall Hangings

The most common shapes for wall hangings seem to be the “S” or wave form in various sizes, and flat pieces of what ever outline supported by stand-offs.

There is another possibility.  You can produce a shallow domed shape which can work well for either landscapes or abstract pieces.  They will be best if circular, although rectangular forms can be used.

The usual resistance to doing this is that the surface will be marked, or that the tack fused surface will be flattened.

There is a way to do this without either effect.  Place the work upside down on a mould of appropriate diameter or dimensions and fire the piece slowly to a low temperature. 

Raise the temperature more slowly than you usually would for a slump in the normal way – top side up.  This allows both surfaces of the glass to be at the same temperature at the same time.  This equalisation of heat throughout the piece will protect against any breaks or splits on the underside of the glass – which will become the top surface.

Set the temperature for about 620C, depending on the span of the piece.  This temperature will be suitable for pieces of 300mm to 400mm and 6mm to 9mm thick.  Pieces with a smaller span will require higher temperatures or longer soaks.  Larger pieces will need a lower temperature.

You should set the soak at about 45 minutes. You will need to observe at intervals until you have the amount of depression you wish.  You will also need to know how to advance to the next segment of the schedule when that point is reached, so that you do not over slump the piece.

Since the piece only touches the mould at the rim, and you are not allowing much movement in the glass, you will not mark the glass with the mould. 

This process of making a domed wall piece will be unusual, although it will not be appropriate in all circumstances.

More detailed information is available in the e-book: Low Temperature Kilnforming.

Large Bubbles

As you move up from smaller pieces to pieces that occupy most of the shelf, you sometimes begin to get large rounded bubbles at tack fuse and burst ones at full fuse.

Image from B Stiverson

You have to go back to basics to discover the cause.

Schedule

It is not likely to be the schedule. It has worked for smaller items. But it is important to review the schedule.  Is it like others you have seen? Is it similar to what the glass manufacturer recommends?  Both these will reassure you that the schedule is OK, if not perfect, or to revise it.

Cleanliness

Going back to the basics relates to the cleanliness of your kiln, among other things.  Even a small speck of material under the glass can result in a bubble. Although the grit lifts the glass off the shelf only a fraction, as it heats up the glass slumps around that and creates an air pocket.  That grows as the glass heats up and creates a large diameter bubble. If there is no grit in evidence, you need to check another element of your kilnforming practice.

Shelf

The large bubble might often occur in the same relative place in the kiln, although different places on the glass pieces, depending where they are placed.  This is an indication that you may have a hollow in the shelf. It may not have been obvious with smaller pieces.  You need to check the shelf with a straight edge. If any light is seen between shelf and edge, you have a depression in the shelf.  It may only be a sliver of light, but that indicates a depression which is enough to create a large bubble. That must be fixed.

Image from Suze

There are temporary and permanent fixes for avoiding bubbles due to depressions in the shelf. 

The temporary fix is to use 1mm fibre paper on the shelf, to allow air out from under the glass.  This can be topped with Thinfire or Papyros. Alternatively, a thin layer of powdered kiln wash can be smoothed over the fibre paper to give the smoothest back possible in the circumstances. You can use a plasterer’s float, or simply a piece of float glass.

The permanent fix is to sand the shelf smooth and level.  A method for doing this is here.

Single Layer Bases

If you are firing with single layer bases, there may be nothing wrong with the shelf.  It is typical in tack fusing to use single layers with glass placed decoratively around the surface of the base.  This leaves gaps where the base glass is exposed.  Even though the whole piece may survive the differential heat up of the exposed base glass and the covered parts, there is the possibility of creating an air pocket under the exposed base.  This comes from the weight of the stacked glass pressing any air out to the side.  If the design is unable to provide a route out for the air, the possibility of creating an air bubble increases.

It is possible to create conditions to reduce the possibility of these large bubbles developing. 

One solution is to use a layer of fibre paper as for a shelf with slight depressions.  This allows air out from under the glass, even with a single layer layup.

The other solution is to change the rate and temperature of the firing.  By using the low and slow principle, you can reduce the risk of bubbles.  Use a much slower rate of advance to a lower temperature with a longer soak you can achieve the look you want without bubbles.  This utilises the concept of heat work.  It does require observation to determine when the effect you desire is achieved and then advance to the next segment.

Further information is available in the ebook Low Temperature Kiln Forming.

Heat Work is Cumulative

“…. the first fuse (contour) I brought it up to 1385°F and held for 5 minutes - it did not contour as much as I would like - do I re-fire at same temp and hold longer or go up in temp and hold same amount of time or something else?”

Observe

Of course, the smart answer is “Observe to get it right first time”.   Observation will enable you to determine when the piece is fully fired.  To observe you need only peek at 5-minute intervals to determine if the piece is as wanted. 

Know your Controller

In combination with this you will need to know your controller well enough to be able to advance to the next segment if the piece is done before the segment finishes; or how to stay on the same segment until it is finished and then advance to the next segment.

Of course, there are circumstance when you cannot or do not want to be present at the top temperature of the firing.  Then consider using the delay function to enable you to be present. This gives a countdown until the kiln starts.  The practice is fully described in this blog entry.

Time or Temperature

If you are experiencing an under-fired piece and want to re-fire it to get a better finish, the usual question is whether to fire for longer or at a higher temperature.

The response is – “Neither”.

Re-fire to the same temperature and time as before, unless you are looking for a radically different appearance.  Heat work is cumulative.  You have put heat into the glass to get the (under fired) result.  By firing it again, the heat will begin to work on the glass as it rises in temperature.  The piece, in this instance, is already a slight contour.  The additional heat of this second firing will begin to work just where the first firing did, and will additionally change the existing surface just as the first firing did.  The degree of contour achieved by the first firing will be added to equally in the second firing.  It is of course, a good idea to peek in near the top temperature to be sure you are getting what you want. More information on heat work is available here with its links. 

Rate of Advance

It is important to remember that on the second firing the glass is thicker, and you need to schedule a slower rate of advance until you get past the strain point – about 540°C for fusing glasses, higher for float and bottle glasses.

Future firings

At the finish of the second firing you will have soaked at the top temperature for twice the scheduled time.  You can use this extra time for the next similar firing, or increase the temperature slightly and keep the original firing’s length of soak. 

As pointed out earlier, observation for new layups, sizes, thicknesses, etc., is important to getting the effect you want the first time.

Low temperature breaks in flat pieces

The usual advice in looking at the reasons for breaks in your pieces must be considered in relation to the process being used.  Breaks during low temperature processes need to be considered differently to those occurring during fusing.  

The advice for diagnosing breaks normally, is that if the edges are sharp, the break occurred on the way down in temperature. Therefore, the glass must have an annealing fracture or a compatibility break.  It continues to say if the edges are rounded it occurred on the heat up, as it broke while brittle and then rounded with the additional heat.

This is true, but only on rounded tack and fused pieces.

I exclude low temperature tack fuses from the general description of when breaks occur in flat pieces as it is not applicable at low temperatures.  

Low temperature flat work includes sintering, laminating, sharp profile tack fusing, etc.  There are lots of other names used for this "fuse to stick" work.  In all these cases, the finished glass edge will be barely different than when placed in the kiln.  It stands to reason therefore that you cannot know when the break occurred, as the edge will be sharp whether it broke on the way up or the way down.  

Periodic observation during the firing is the only way to be sure when the break occurred. These observations should coincide with the move from the brittle to the plastic stage of the glass.  Therefore, about 540C.  It can be at a bit lower temperature, but not a lot.  If the glass was not broken by that time, you can be fairly certain it broke on the way down.

Further information is available in the ebook Low Temperature Kiln Forming.

Getting the Right Firing Temperature

“what temperature should I use to get a tack fuse that is just less than a contour fuse?”

This is the kind of question that appears on the internet often.  Unfortunately, no one can answer the question accurately, because it depends on some interrelated variables.

Kiln characteristics

Top or side elements, size of kiln, relative size of piece, all have an effect. Also no two kilns even of the same model have exactly the same characteristics.

Ramp Rate 

How quickly or slowly you fire has a big effect on the temperature and soak needed to achieve the desired result. This is the effect of heat work.

Temperature

There are no absolute temperatures for a given effect, given the above two variables.

Soaks

The length of time and the number of soaks will affect the temperature required to achieve your effect.

OK. So, what can I do?

Observation

The only certain way to get the effect you want is to observe.

Set a schedule, guessing the top temperature and length of soak.  Know your controller well enough that you can extend the soak or end the segment by advancing to the next.  Your manual will tell you how to do this.

Peek at intervals from 10-15C below the selected target temperature. Peek at 5min intervals until the effect is achieved.  Advance to the next (cooling) segment.  Record the temperature and length of soak at which the effect was achieved.  On subsequent firings you can experiment with reducing the temperature by 5C – 10C with a 10-minute soak.  Observe and record the temperature and effect as before.

The reason for going for a 10-minute soak rather than longer is to avoid holding at the target temperature for a long time, as that can help induce devitrification.  The reason for a soak at all is to achieve the minimum of marking on the reverse or picking up kiln wash or kiln paper on the back.

If effect is not achieved by the end of the soak, extend it by using the appropriate key or combination of keys.  Keep observing at five-minute intervals until the effect is achieved.  Advance to the next segment and record both the temperature and time.  The objective is to get the heat work done with a 10-minute soak, so you will need to increase the temperature on the next firing.  The amount of increase will depend on the length of soak required to get the desired surface on the previous firing.  The longer the soak, the more temperature you need to add.  You will need to repeat the observations and recording until you find a temperature that will achieve the effect with a 10-minute soak.

Use the lessons from the observations to lower temperature, extend soak, raise temperature, reduce ramp speed, or reduce soak as required.  It will also help you judge on other pieces the approximate temperature and time required for the new layups or new moulds.

Slumping unknown glasses

I had a recent request for help from an old friend who has taken up kiln formed glass. The problem is common enough, that (with her permission) I am adding it to the tips section.

I tried an experiment today to use some of my nice (non-fusing) glass. I cut at 270 mm diameter circle from a 3mm thick sheet and wanted to slump it into my 270 mm bowl mold. I set the mold up carefully and checked it was dead level in all directions and that the glass was absolutely centered on it. I have no idea what the COE is so decided just to use the S96 recommended slumping temperature of 650C. When I checked the kiln no more than 2 minutes after it had reached 665C, the glass had slumped almost to the bottom of the mold but it had slumped very asymmetrically. There was also a small burp on one side which has never been an issue when slumping bowls in this mold before.

The schedule I used was as follows:
200C/hour to 540C, 0 hold
650C/hour to 665C, 10 hold
Then standard S96 anneal programme

Also, the edges were still a bit rough from the cutting, i.e., they hadn‘t fire polished at all. Can you help?

Finding out about the softening characteristics of the glass

Slumping a single layer of glass with unknown characteristics – the CoE is not really relevant – requires that you watch it and other similar ones until you have established a slump temperature for the glass.

There is a way to do it:
Cut a piece of glass 305mm long by 20mm wide. Support it 25mm above the kiln shelf with the posts being 290mm apart. Put kiln furniture on top of the glass where it is supported. Make sure you can see the shelf just under the middle of the suspended glass when you are setting up this test. You can put a piece of wire or other dark element there on the floor of the kiln to help you see when the glass touches down.

Set the kiln to fire at 100C/hour to about 680C. Peek at the suspended glass every 5-10 minutes after 560C to see when the glass begins to move. Then watch more frequently. If your kiln has an alert mode on it, you could set it to ring at each 5C increase in temperature, otherwise use an alarm that has a snooze function to make sure you keep looking. When the glass touches down to the witness sitting on the shelf, record the temperature. This will approximate the slumping temperature in a simple ball curve mould.


Getting smooth edges

You need to have smooth edges before slumping. You can fire polish the piece of glass to get rounded edges, or you can cold work the edges with diamond hand pads, working from the roughest to the finest you have available. If that does not give you the edge you want, you will need to fire polish before you try to slump.

You can do at least two things to find the fire polish temperature. You can do a little experiment by using the cut off pieces of the glass and roughing them up a little before putting in the kiln. Make sure you can see it through the peep hole(s). Set the kiln to fire at about 250C to say 750C. Look in from about 700C to determine when the edges begin to round.

The other is to put a strip of the same glass in with the slump test and set the kiln to go up to 750C rather than just 680C. You can check on progress just as for the separate firing to determine the fire polish temperature. I think about 40C above slump temperature should be enough, but your test will determine that.


Avoiding uneven slumps

Most uneven slumps occur because of too fast a rate of increase in temperature. The piece can hang up on the mould sometimes causing the glass elsewhere to slide down to compensate. The real difficulty in the schedule was the 650C/hour rate up to the top temperature. This was so fast that the glass at the edges would have the opportunity to soften and so hang before the centre was soft enough to begin to bend. 150C / hour would be fast enough from 540C to achieve the slump.  In fact, 150C/hour all the way to the slumping temperature would be fast enough.  The glass reacts well to a steady input of heat rather than rapid rises, even with soaks at intervals on the way up.

Other things can be done too. You mentioned the edges were rough from the cutting. This can cause difficulties of hanging. To avoid that, you should smooth the edges before placing the glass on the mould. A further precaution against uneven slumping is to give a slight bevel to the bottom edge so that it can slip more easily along the mould.

You had already done the leveling of the mould and the centralization of the glass on the mould. These are two other things that can cause uneven slumps.


Avoiding “burps”

The glass slipping a long way down the mould is often accompanied with burps or bubble like up-wellings. These are both indications of too high a temperature being used to slump. I would begin looking at the glass from about 600C in the slumping of any unknown piece of glass. That would apply to any new configuration of the glass or mould too. The fact that the glass slid to the bottom and had a burp means that the temperature was too high and too fast. Once you have established the lowest slumping temperature, by watching to see when it begins, you then can add about 30 minutes soak to that temperature. The length of this soak will have to be determined by observation and experience, though.

A slow heating allows the glass to be at an even temperature throughout its thickness. A rapid rise with a thick piece will sometimes reveal a tear like opening on the underside of the glass that does not come through to the top. This is because the upper surface is sufficiently hot to begin slumping while the bottom is just a little too cool. If there is too great a difference, the glass just breaks all the way through.

Also slow heating allows the slump to be accomplished at a lower temperature, leading to fewer problems and to less texture being taken up from the mould.

More detailed information is available in the e-book: Low Temperature Kilnforming.