Friday, 7 February 2025
Float Annealing Temperatures
Monday, 30 December 2024
Slump Point Test
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The 305mm strip suspended 25mm above the shelf with kiln furniture. |
Place some kiln furniture on top of the glass where it is suspended to keep the strip from sliding off the support at each end. Place a piece of wire under the centre of this span to make observation of the point that the glass touches down to the shelf easier.
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The strip held down by placing kiln furniture on top of the glass, anchoring it in place while the glass slumps. |
If you are testing bottles, you may find it more difficult to get such a long strip. My suggestion is that you cut a bottle on a tile saw to give you a 25 mm strip through the length of the bottle. Do not worry about the curves, extra thickness, etc. Put the strip in the kiln and take it to about 740C to flatten it. Reduce the temperature to about 520C to soak there for 20 minutes. Then turn the kiln off.
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The completed test set up with an annealing test and wire set at the midpoint of the suspended glass to help with determining when the glass touches down. |
The schedule will need to be a bit of guess work. The reasons for the suggested temperatures are given after this sample initial schedule which needs to be modified during the firing.
Ramp 1: 200C per hour to 500C, no soak
Ramp 2: 50C per hour to 720C, no soak
Ramp 3: 300C per hour to 815C or 835C, 10 minute soak
Ramp 4: 9999 to 520C, 30 minute soak
Ramp 5: 80C per hour to 370C, no soak
Ramp 6: off.
In Fahrenheit
Ramp 2: 90F per hour to 1328F, no soak
Ramp 3: 540F per hour to 1500F or 1535FC, 10 minute soak
Ramp 4: 9999 to 968F, 30 minute soak
Ramp 5: 144F per hour to 700F, no soak
Ramp 6: off.
Fire at the moderate rate initially, and then at 50C/90Fper hour until the strip touches down. This is to be able to accurately record the touch down temperature. If you fire quickly, the glass temperature will be much less than the air temperature that the pyrometer measures. Firing slowly allows the glass to be nearly the same temperature as the air.
Observe the progress of the firing frequently from 500C/932F onward. If it is float or bottle glass you are testing you can start observing from about 580C. Record the temperature when the middle of the glass strip touches the shelf. The wire at the centre of the span will help you determine when the glass touches down. This touch down temperature is the slump point of your glass. You now know the temperature to use for gentle slumps with a half hour soak. More angular slumps will require a higher temperature or much more time.
The next operation is to set this as the annealing soak temperature in the controller. This will be the point at which it usually possible to interrupt the schedule and change the temperature for the annealing soak that you guessed at previously. Sometimes though, you need to turn the controller off and reset the new program. Most times the numbers from the last firing are retained, so that all you need to do is to change the annealing soak temperature.
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Squares of glass showing different levels of stress from virtually none to severe (no light emanating for no stress to strong light from the corners indicating a high degree of stress.) |
- Of course, before doing any other work, you should check your arithmetic to ensure the calculations have been done correctly. I'm sure you did, but it is necessary to check. If they are not accurate, all the following work will be fruitless.
- The observation of the touch down of the suspended strip can vary by quite a bit - maybe up to 15C. To check this, you can put other annealing test pieces in the kiln. This will require multiple firings using temperatures in a range from 10C/18F above to 10C/18F below your calculated annealing soak temperature to find an appropriate annealing soak temperature.
- If stress is still showing in the test pieces after all these tests, you can conduct a slump point test on a strip of glass for which there are known properties. This will show you the look of the glass that has just reached touch down point as you know it will happen at 73C above the published annealing point. You can then apply this experience to a new observation of the test glass.
Breaks after the Piece is Cool
Thermal Shock
If the break occurs after the piece is cool, it is not thermal shock.
Annealing
Another possible cause of delayed breakage is inadequate annealing. Most guidelines on annealing assume a flat uniform thickness. The popularity of tack fused elements, means these are inadequate guides on the annealing soak and annealing cool. Tack fused items generally need double the temperature equalisation soak and half the annealing cool rate. This post gives information on how the annealing needs modification on tack fused items.
Compatibility
- Compatibility is much more than the rate of expansion of glass at any given temperature.
- It involves the balance of the forces caused by viscosity and expansion rates around the annealing point.
All is not lost. It does not need to be left to chance.
If you are buying by CoE you must test what you buy against what you have.
Do not get sucked into the belief that CoE tells you much of importance about compatibility.
Wednesday, 27 March 2024
Kilnforming Opalescent Stained Glass
The statement that
a sheet of glass can be fused to itself is true in certain circumstances. It applies to transparent and some streaky
glasses best. These forms of glass are more
likely to fuse together successfully although not formulated for fusing.
Transparent and Streaky Glasses
Of course, the best practice is to test for compatibility. I found in my early days of sticking stained
glass together that it was beneficial to test. In doing so, I found Spectrum
and Armstrong transparent and streaky glass to be largely consistent across
many sheets. I did not have access to much
Kokomo or Wissmach. I cannot comment on
how their glass behaves in terms of compatibility across the production range. Not all transparent and streaky glass remains
stable at fusing temperatures. There are
some glasses that opalise, some change colour, some devitrify. This variability makes compatibility testing
important - even for the transparent form of stained glass.
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Photo credit: Lead and Light |
Wispy Glasses
The statement
about fusing to itself is less applicable to wispy glass. Not all the wispy stained glass from the same
sheet can be fused. It seems to be
dependent on the amount of opalescence in any one area of the glass. I found that it is possible - if you are very
careful - to fuse certain Spectrum wispies with the clear fusing standard on
top, but not on the bottom. This should
be applicable to other manufacturers’ wispy glass too. There must be a marginal compatibility that
is contained by the clear fusing glass on top, but I am not certain.
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Photo credit: Lead and Light |
Opalescent Glasses
The statement about
fusing to itself is almost completely inapplicable to opalescent glass. Stained glass opalescent glass does not have
the compatibility requirements of fusing glasses. They very often severely devitrify when taken
to fusing temperatures. This
devitrification means that opalescent stained glass is often not compatible
with itself. So, no amount of twiddling
with schedules will make stained glass opalescent glass fusible, even with
itself.
Manufacturers have
spent a lot of time and effort to produce fusing compatible opalescent glass. It is as though there is a minor element of
devitrification embodied in the opalising process. Whether this is so, it becomes very apparent on
doing compatibility testing that opalescent stained glass has severe devitrification
at fusing temperatures.
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Stock photo |
Compatibility Testing
It is important to
test for compatibility before committing to the main firing. Some transparent and streaky glass changes
colour, devitrifies, and some opalise at fusing temperatures. This applies with
even more force to wispies. They contain
a significant proportion of opalescence within them. Some opalescents are so unstable at fusing
temperatures that the devitrification becomes so bad the glass crumbles.
The importance of
testing pieces of the sheet for compatibility before committing to a firing is
reinforced by these factors.
Slumping
Slumping temperatures
are not so high as fusing, and it is often stated that single layers can be
slumped. Again, it is not always true.
Some glasses
change colour at slumping temperatures. A few opalise. It is not always certain what effect moderate
temperatures will have on stained glass. The compatibility testing will show. Observe the test firing at slumping
temperatures. Also, you will learn if
there are changes at moderate temperatures.
One element must be commented upon about slumping. It is important to have the edges finished to the appearance that you want the final piece to have. The regularity of the edges without bumps or divots, and the degree of polish need to be showing before the firing starts. The slumping temperatures are not high enough to alter the shape or appearance of the edges.
Firing of stained
glass to itself is normally a low risk activity, but with unpredictable results.
It can teach a lot about behaviour of
glass at higher temperatures. Slumping
single layer pieces can give information about the way single layers of glass
slump or drape. But testing is important
for fusing. And can inform about how the
glass will react at slumping temperatures too.
Sunday, 27 August 2023
Coe and compatibility
- ·
The coefficient is for an
inappropriate temperature range for glass.
- ·
The
critical temperatures for expansion are in the annealing range, for which there
are no widely published figures.
- ·
The
expansion rates need to be adjusted to match the viscosity in this annealing
range.
- ·
A
major manufacturer has indicated their glass, known by the CoE of its fusing
standard glass, has a 10-point range of CoEs within their fusing range.
Compatibility of Glasses with the Same CoE
CoE Useage
The temperature range used is 20C to 300C. Expansion characteristics vary greatly at higher temperatures.
Whether you call it CoE or CoLE is immaterial, as it still does not equal compatibility.
It does measure expansion rates, but up to 300C only. It does not tell you how glass expands above that temperature. Note: it does not behave in a linear pattern as crystalline materials do.
"CoE Equals Compatibility" - Kiln Forming Myths 10
Other posts on Compatibility are here:
Is Coe Important?
What is Viscosity?
CoE varies with temperature
Defining the glass transition stage