Multiple Firings of Kiln Wash

Many people report that they fire multiple times on kiln wash that has not been renewed.  Most add coats over existing kiln wash.  They only remove all the kiln wash when it begins to crack, stick to the glass or gets divots.

We all know that kiln wash fired a second time to full fuse is likely to stick to the glass.  We also know that kiln wash fired to slumping temperatures lasts almost indefinitely.  The kaolin in the kiln wash that allows easy spreading, undergoes a gradual change from platelets to crystals with increasing temperature.  This begins at around 600C/1115F and is complete by 900C/1655F.  The crystalline version of kaolin sticks kiln wash to glass, but as the transition from platelet to crystal is so slow at the lower end of the range, kiln wash on slumping moulds does not exhibit the sticking behaviour even over very many firings.  But, as the temperature rises, the risk of there being enough crystals to stick the kiln wash to the glass also increases.  By full fuse temperatures the proportion of crystalline kaolin is high and becomes complete on the next firing.

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credit: Immerman Glass

It is possible to fire several times to tack fusing temperatures without experiencing the sticking behaviour of kiln wash.  However, the more times and the higher temperature used, the greater risk of kiln wash sticking.

Some people continue firing without adding additional layers of kiln wash until cracks, divots, or sticking occurs.  This leads to creating a fix after the failure of the kiln wash. This requires both finding a means of cleaning the kiln wash residue from the glass, and fixing the firing surface.

Others paint a layer of kiln wash on top of the existing separator before high temperature firings. This continues each firing with a fresh layer of kiln wash.  However, the same cracks, divots, and sticking occurs at some point, requiring a complete re-coating of the shelf, and getting the kiln wash off the glass.

credit: Sue McLeod Ceramics

Re-coating of a shelf takes a couple of minutes and can be done with simple tools.  A broad scraper will remove most of the kiln wash.  This can be followed by rubbing with an open weave sanding sheet as used for plaster board or other dry walling.  If you are worried about the dust – which has less risk than fibre papers – you can dampen the surface before beginning the cleaning process.

If the kiln wash has been on the shelf for many firings, it is more difficult to remove, requiring more effort than a single firing.  High temperature firings as for melts also make the kiln wash more difficult to remove. But the same process is used in these cases.

       

Kiln wash in firings at slump and low temperature tack fuses can be reused as many times as it remains smooth and undamaged since the temperature is not high enough to cause the chemical changes.

The ultimate benefits of renewing kiln wash are that not only less effort is required to clean and re-coat, than to fix pieces, and also the cost of kiln wash is significantly less than fibre papers.

Removing kiln wash

Applying kiln wash

Revisde 18.1.25

Spider Web Cracks

 

Credit ASTM

 The nature of the cracks - and spider web describes it perfectly - shows an adhesion problem. It is not an annealing problem as that shows a single sinuous line with a hook at each end. It is not a compatibility problem, as that shows as cracks or breaks along the edges of the combined glasses. It is not a thermal break, as those show as breaks where the glass has separated to some amount.

 

Glaze crazed in a ceramic vessel

 

The cracks are exactly like crazed glazes on ceramic objects. And for the same reason. The glass is trying to contract more than the underlying ceramic. It is stuck to the pores of the ceramic and creates a crack where there is a slightly weaker part of the glass. These cracks in ceramic glaze propagate across the surface as it wears, or in the kilnforming case as it cools.

 

Glass puddled in ceramic

 Most usually it results from a lack of separator in that area of the shelf, or uncoated kiln furniture. It indicates either the glass has adhered to the shelf or mould, or (rarely with fusing glass) that the glass has suffered severe devitrification.

 

 

 Occasionally there will be the appearance of shards of glass. This will be where the glass has stuck to some particle on the shelf. Sometimes it can be a speck of something resistant to the temperatures we use in kilnforming that “grabs” the glass and breaks it into shards from that point as the glass cools.

 It is not the schedule that causes the breaks. It is in the shelf preparation.

 The shelf should be cleaned of all the kiln wash and lightly sanded down to smooth. It should then be coated with four thin layers of kiln wash painted in a different direction for each layer. No drying is necessary or even advisable. All kiln furniture must be completely coated with kiln wash.

 If you are re-using a shelf, it must be swept clean before any glass is laid on it.

 Crazing results from the glass sticking to the surface it is resting on.

 

Some additional information:

https://glasstips.blogspot.com/2019/05/kiln-cleanliness.html

https://glasstips.blogspot.com/2020/07/crazing.html

 

Drying Kiln Washed Moulds

A question about kiln wash. Do you have to let each coat dry while applying before applying the next coat?

 There seems to be a popular notion that newly kiln washed moulds must be cured before use.  I'm not sure where the information comes from, and no reasoning is given.  It is suggested that that quickly heating newly kiln washed moulds to 550°F (290°C) is important.

 If you want to make sure the mould is dry, this may not be the best way to do it.  All ceramics have a cristobalite inversion at around 225°C/437°F.  This a very rapid increase in volume of 2.5% that often leads to cracks and breaks in ceramics when the rate of advance is quick.  The mould will react better and last longer if the rate of advance is slow until that inversion temperature is passed.  But also note there is a quartz inversion at around 570°C/1060°F that is significant.

 

 This is another reason to advance the temperature slowly when slumping or draping with a ceramic mould.  A further reason to heat slowly is to avoid steam formation within the ceramic body.  If the steam is created over a short time, the force can be great enough to break the ceramic.  To ensure the water evaporates, a soak at 95°C/203°F for a significant amount of time is a better, safer option.

 But in addition to all these precautions, it simply is not necessary to cure kiln wash on slumping and draping moulds made of ceramics.  The glass does not begin to move until after 540°C/1000°F. Therefore, the kiln wash will be dry long before the glass gets near slumping temperatures.  Any vapor caused by evaporating water will escape through the vent holes in the mould or under the glass at the rim, as it will not form a seal until higher temperatures.

 

Newly kiln washed mould beside others already fired

 If you want to be sure your kiln wash is dry before you put the mould in the kiln, you can leave it in a warm ventilated space, or even on top of your kiln while it is being fired.  Using either drying method will dry the kiln wash sufficiently before the glass is placed on the slumping mould.

 The other part of the question was about drying the kiln wash between applying coats. It is not necessary to dry between coats of kiln wash.  In fact, a better result is obtained by applying all the coats at one time. It is not like painting wood. The result of applying all coats is a smoother surface.  There is no dragging of the dry powder along with the wet kiln wash as it is being applied over the existing coats.

 Kiln drying ceramic slumping and draping moulds is not necessary. It only adds another, unnecessary step in kilnforming preparations.  There are exceptionally good reasons to avoid rapid firing of damp moulds. 

 Some extra care could be taken with texture moulds and those intended for casting.

Calibrating your new kiln

My new kiln fires differently than my existing one(s).

Each kiln will be different in minor or major ways.  Suggested schedules are only starting points, even though they worked in your previous kiln. You need to learn about your new kiln’s characteristics in the same way you did with your first kiln. There are a number of ways to do this.

Many people recommend making test tiles for the different levels of fusing that you use and at different temperatures to determine which is the best for your new kiln.  Additionally, you need to note the rate(s) at which you fired these samples to make the test tiles accurate representations of firings.  Yes, these will be good references.  And yes, they are valuable if you have the time for all these firings.

 Idle Creativity

Observation during the firing of test tiles is the best and quickest way to discover how your new kiln is performing at various temperatures.  In one firing you can note the temperatures at which the various tack levels occur, and the contour and full fuse temperatures.  You can even take pictures through the peep hole of your kiln (as long as you don’t put the camera too close to the kiln!).  This procedure will make knowing your kiln much quicker and accurate than unobserved multiple firings.

To make use of the notes of the temperatures where the results were achieved in the test firing, back off 10°C (or 20°F) from the observed temperature and add 10 minutes processing time.  You may find after a few uses of these temperatures you may want to adjust the temperature a bit more, but you will have done the major experimental work in one firing.

It is a good idea to set up other test tiles and run the experiment again at a slower rate of advance.  This will give you information about how the different rates of advance affect the processing temperature and the look and texture of the piece, especially on the bottom.  The texture imparted at different processing temperatures becomes more important in slumping and draping processes.

In another firing you can set up various moulds and observe when the slumps or drapes are complete. Recording this information lets you know slump temperatures for various styles and spans of moulds.  Make sure you record the temperatures that the pieces slump fully into the mould. You can then back off 20°C from those points and add 30 minutes as a starting point for you actual slumping firings.

New kilns require experience to know what the appropriate temperatures are.  Buy setting up test tiles you can observe in one firing the various levels of fuse from tack to full fuse, so saving lots of firing time.

Further information is available in the ebook: Low Temperature Kiln Forming.

Large Bubbles

As you move up from smaller pieces to pieces that occupy most of the shelf, you sometimes begin to get large rounded bubbles at tack fuse and burst ones at full fuse.

Image from B Stiverson

You have to go back to basics to discover the cause.

Schedule

It is not likely to be the schedule. It has worked for smaller items. But it is important to review the schedule.  Is it like others you have seen? Is it similar to what the glass manufacturer recommends?  Both these will reassure you that the schedule is OK, if not perfect, or to revise it.

Cleanliness

Going back to the basics relates to the cleanliness of your kiln, among other things.  Even a small speck of material under the glass can result in a bubble. Although the grit lifts the glass off the shelf only a fraction, as it heats up the glass slumps around that and creates an air pocket.  That grows as the glass heats up and creates a large diameter bubble. If there is no grit in evidence, you need to check another element of your kilnforming practice.

Shelf

The large bubble might often occur in the same relative place in the kiln, although different places on the glass pieces, depending where they are placed.  This is an indication that you may have a hollow in the shelf. It may not have been obvious with smaller pieces.  You need to check the shelf with a straight edge. If any light is seen between shelf and edge, you have a depression in the shelf.  It may only be a sliver of light, but that indicates a depression which is enough to create a large bubble. That must be fixed.

Image from Suze

There are temporary and permanent fixes for avoiding bubbles due to depressions in the shelf. 

The temporary fix is to use 1mm fibre paper on the shelf, to allow air out from under the glass.  This can be topped with Thinfire or Papyros. Alternatively, a thin layer of powdered kiln wash can be smoothed over the fibre paper to give the smoothest back possible in the circumstances. You can use a plasterer’s float, or simply a piece of float glass.

The permanent fix is to sand the shelf smooth and level.  A method for doing this is here.

Single Layer Bases

If you are firing with single layer bases, there may be nothing wrong with the shelf.  It is typical in tack fusing to use single layers with glass placed decoratively around the surface of the base.  This leaves gaps where the base glass is exposed.  Even though the whole piece may survive the differential heat up of the exposed base glass and the covered parts, there is the possibility of creating an air pocket under the exposed base.  This comes from the weight of the stacked glass pressing any air out to the side.  If the design is unable to provide a route out for the air, the possibility of creating an air bubble increases.

It is possible to create conditions to reduce the possibility of these large bubbles developing. 

One solution is to use a layer of fibre paper as for a shelf with slight depressions.  This allows air out from under the glass, even with a single layer layup.

The other solution is to change the rate and temperature of the firing.  By using the low and slow principle, you can reduce the risk of bubbles.  Use a much slower rate of advance to a lower temperature with a longer soak you can achieve the look you want without bubbles.  This utilises the concept of heat work.  It does require observation to determine when the effect you desire is achieved and then advance to the next segment.

Further information is available in the ebook Low Temperature Kiln Forming.

Kiln Maintenance

Switch off the kiln before doing any maintenance.

Before or after each use

Vacuum the inside of the kiln. Use a low suction setting, especially on fibre walls and ceilings. Stronger suction is possible when cleaning a brick floor.

Example of vacuuming around elements

Example of vacuuming lid without elements

An alternative to vacuuming the elements is to use the air compressor hose at low power to gently blow out any dust settled in the element grooves.  Do not do this for fibre insulated kilns, only brick.

Check on the kiln furniture – including shelves, boards, supports. Are they kiln washed and without scrapes, scratches, gaps? Has the kiln wash been fired to full fuse temperature? In both cases, clean the used kiln wash off the shelf and renew.

Check that the shelves and other kiln furniture are without cracks.

Clean kiln furniture of dust and debris.

Check the level of any item newly placed in the kiln - e.g., mould, or shelf replacement - with a spirit level.

Two examples of two-way spirit levels

 Check on the conditions and placement of the thermocouple.

Check on the elements.  Some may be sagging or hanging out of their channels.  Use tweezers to bring the coils closer together.  This shortens the length of the element and it then can be pushed back into the channel.  It may not have to be done after each firing, but checking will catch things before sagging becomes a major problem.

When the shelf paper is exhausted lift out the thicker papers and vacuum the shelf.  The Thinfire and Papyrus papers can be vacuumed directly or gently swept up and placed in a container for disposal.  Do not introduce any moisture to help reduce the dust.  This is not good for the kiln or you, as it could induce shorting out of the elements.

Monthly

Electrical parts: check the elements and their connections (normally at back or side).

First unplug or switch off the power to the kiln.

Check the screws on the connectors for the element tails are tight. Loose connections cause the wire to vibrate at the connection during the power phase. They heat up enough to melt the wire at the connection. For a single element kiln, it will simply lose power.  In multiple element kilns the remaining elements work much harder to achieve the temperature and provide uneven heating.

If the connectors are badly corroded , they need to be replaced.  This can be done without replacing the elements. Unscrew the connectors and put new ones on.  If the connector is fused to the element wire, you need to cut the wire as close to the connector as possible to maintain a length of wire for the new connector to be fixed.

Check the condition of leads and plugs supplying power to the kiln.  Make sure they are sound, not frayed and not kinked. Replace any frayed parts.  Take out any kinks in the power supply cable.

Any support pins or wires should be firmly seated in the brick work or supported by sound hangers.

Check the level of the kiln floor and internal shelves on a regular basis and every time the kiln and its internal furniture is moved.

Making a schedule of maintenance checks and noting on it the dates checked is a good idea for those who need reminders.

Bubble Mystery

A question was asked about a collapsed bubble. There were two pieces in the kiln and one (strips) was fine and the other (flat plate) had the collapsed bubble.  Both on the same dried shelf.  The question also asked if the collapsed bubble piece could be flattened by fusing again.

Collapsed Bubble

The bubble collapsed because it had not burst by the time the cool toward annealing had begun.  As the air pressure under the bubble dropped, and the weight of the thinned glass bubble sank down as there was not enough air pressure to hold it up.

The glass is now thinner at the centre of the bubble than the main part of the piece, and thicker at the edge of the bubble. I don't think it is possible to successfully flatten it to become an even thickness across the whole piece. To get the same thickness across the whole piece would require high temperatures and long soaks there. 

Another possibility is to use a pressing solution. 

My suggestion is to add elements or repurpose it. I don’t think any repairs would present a good-looking piece.

Diagnosis

The on-line diagnosis of the possibilities for the cause of the bubble was extensive and sometimes inventive.  It was finally determined the bubble was from under the glass, that is, between the glass and the shelf. A slight depression in the shelf is the usual explanation.  The user tested the shelf for smoothness and found no depressions.

It was clear the bubble came from under the glass.  All the suggestions about how bubbles can form under glass were given, but none seemed to apply.

How can you get a bubble on a dry shelf that is perfectly flat and that has not been subjected to too rapid or too high a temperature?

Solution

The answer is that a little spot of grit or tiny ball of fibre paper can keep the glass raised up enough for air to be trapped.

Prevention

It is not enough to test the shelf is flat.  You need to use clean kiln wash with a clean brush to avoid any grit being brought to the shelf. It is also a good reason to vacuum the shelf before each use in case any dust or grit has fallen onto the shelf. Covering the shelf or putting it into a cupboard will also reduce the possibility of small bits of grit falling onto the shelf.

Of course, if you smooth the kiln wash with a nylon or similar fine cloth, you will remove any specks of grit.  A vacuum of the shelf after smoothing is still a good idea.

Conclusion

It is as important to keep tools and materials clean as it is to clean the glass you are going to kilnform.

Sand Beds for Kilns

Sand beds can be used for shaping directly into the sand or as a bed for a large kiln to avoid having to place a number of shelves together and patch cracks. It also saves on the purchase of a large shelf, at the expense of some labour before each firing.

Mix (by weight)

The mix is largely sand with powders to coat the sand particles to reduce the amount of sticking to glass. The mix ranges from 75% sand 25% alumina hydrate, up to 67% sand, 33% alumina. The proportions can be adjusted by experience.

Some kiln formers include plaster or china clay (kaolin) in various proportions so the whole mix can range from 70% sand, 25% alumina, 5% plaster/kaolin up to 60% sand, 20% each alumina and plaster/kaolin. Some have found that the plaster started to scum up the glass after a number of firings, and this can happen with china clay too.

Use

The use of sand as the bed of the kiln requires screeding of the sand before each firing. It is possible to smooth the sand with a plaster’s float. This presses the sand down and allows a fine film of powder to coat the surface. A more certain way of avoiding the sand sticking to or texturing the glass is to lay fibre paper over the sand.

You should be aware that a sand bed requires a little different cooling than glass on a suspended shelf does. Effectively you are cooling the glass on the bed of the kiln. Thus, you should use annealing and cooling schedules for one or two thicknesses more than is actually being fired to be really safe.

Sand forming

If you are using the sand for mild shaping, sprinkle alumina hydrate over formed sand to reduce sand particle take up and textures onto the glass.

Renew sand regularly if you are using powders on the sand. An annual renewal using half the old sand mix and the rest new will be sufficient in most cases. The effect of too much powder is to promote large bubbles as air cannot move through the sand with the same ease as when there is less powder. An easy way to tell if you have too much powder is that the mix flows ahead as you screed it.

Revised 22/6/19

Applying kiln wash

Applying kiln wash to shelves and moulds have the same requirements.

The kiln wash must be applied evenly

You can use a soft bristled brush like a hake and trail on the kiln wash in four directions – top to bottom, side to side, and diagonally left to right and right to left.

The pigmented kiln wash turns white when fired

You can also spray the kiln wash onto the shelf or mould. This can provide an even coating, but you must be careful to avoid puddling the kiln wash. Pause for a few seconds after each coat to allow the water to be absorbed before applying the next coat. Apply until the shelf or mould surface is not obvious through the kiln wash. There is no need to dry between coats.  The best coverage is achieved by applying all four coats in different directions at the same time.

You can use a sponge to apply to flat surfaces. A light touch is required and it needs to be apply in various directions as with the brush.    

Metal moulds are a special case. The water carrying the kiln wash will simply bead up or run off the metal. First clean the metal to get rid of oils and dirt – sandblasting will do well. Then you need to heat the metal to about 125C – 150C (i.e., above boiling) and brush or spray the kiln wash onto the mould, one coat at a time. Return the mould to the heat source and then apply another coat of kiln wash. Do this until you have an even layer of kiln wash. Be careful not to put so much liquid on the mould that it begins to run. If this happens, you really need to start again.  Also if the metal is too hot, the water will boil off, leaving bare patches.

Apply the kiln wash thinly

You need enough kiln wash to separate the glass from the carrying surface. Any additional kiln wash will not make for a better separation, but may begin to flake off the surface and adhere to the glass more or less tightly.

The usual recommendation for brushing is one part kiln wash to five parts water. I recommend ten parts water to one part kiln wash if you are spraying the kiln wash. If you have a really absorbent surface, such as a vermiculite mould, you can reduce the water to two and a half parts water to one kiln wash. All these measurements are by volume.

The kiln wash finish must be smooth

There are several ways to smooth the surface.

You can rub your hand over the shelf or mould to remove high spots/streaks. You need to remove the dust before using though.

You can smooth the surface using a rolled up nylon stocking. This relatively open weave allows the powder to be captured in the material. It works well on irregular surfaces like a mould. Again you must clear off any remaining dust.

Another way is applicable to flat surfaces. After applying the kiln wash, but before it has dried, make sure the surface is level. Then brush or spray on a layer of hot water. This both puddles and evaporates quickly, leaving a smooth surface on thinly applied kiln wash. If the kiln wash is thick, the drying process will leave cracks as in a dried-out river bed.

Kiln Washing Kiln Surfaces

“Having just got my first kiln, I was wondering how often I have to add kiln wash to the bottom of the kiln.”

It has become common practice to kiln wash the bottom of a new kiln.

This may be fine for brick lined kilns.  Kilns with fibre blanket or fibre board do not need to be kiln washed at all.  The fibre is a separator already and does not need additional material which will turn to powder and need to be carefully cleaned to avoid damaging the refractory fibre lining.  This has led me to reconsider the value of kiln washing the bottom of the kiln.

I have followed the practice kiln washing of the bottom of the kiln in the past.  However, I have found that small glass pieces falling to the floor, do not stick to the bare brick or to fibre.  They can be vacuumed or picked from the surface of the kiln without creating any damage.  This means that at fusing temperatures, the brick and fibre does not stick to the glass and kiln wash is not needed.

The main idea seems to be to help protect the kiln surfaces from the molten glass if a relay becomes stuck, raising the kiln temperature to very high levels. Kiln washing the bottom of the kiln does not protect the brick or fibre from a large amount of glass running off the edge of the shelf onto the bottom. Of course, pieces of glass resting on the floor of the kiln may become stuck when higher temperature work is being conducted, such as combing, the various melts, and casting.  The solution is not to kiln wash the floor, but to clean the floor of the kiln before entering the high temperature processes.

There is not really a need to kiln wash the bottom of the kiln at all.  The kiln wash will not protect the kiln brick or fibre in the event of a high temperature accident.  The kiln wash turns to powder which needs to be cleaned from the kiln to avoid contamination, as with other dusts, of the glass being fired.  The main objective is to keep the kiln clean and free of dust rather than adding another source of dust.  A dusty atmosphere in the kiln can promote devitrification, so anything which avoids introducing dust will be beneficial in reducing the incidence of devitrification.

I suppose if you really want to protect the bottom of the kiln from molten glass, you can add a high temperature separator such as a refractory fibre board, or a thin layer of sand.  The sand will resist the molten glass and can be scooped out of the bottom before adding new. 

After some consideration, I no longer think kiln washing the bottom of kilns is worth the potential for dust accumulation, as it doesn’t really protect the kiln floor during high temperature accidents. Low temperature spills of frit, glass powder and shards will lift off the kiln surfaces easily without damage to surfaces.

Kiln Cleanliness

Problems with finished pieces can be caused by an untidy or dusty kiln interior.  Pieces can be affected by devitrification or specks of refractory material in or on the fired project.

Dust is a common problem.  Kiln wash, fibre papers and combustion products all produce particles that are collectively referred to as dust.

Vacuuming the kiln regularly is a good practice to keep the dust down.  It is best if the vacuum has a variable suction control to avoid damage to the refractory materials which make up the kiln.  It is best to use a brush attachment rather than the bare hose.

Dust on the brick or fibre board floor of kilns can be vacuumed easily if you remove the shelf.  Usually you need to use the most suction available to pick up heavier particles such as glass frit along with the dust that accumulates on the floor.

Dust also accumulates on the sides and top of the kiln too.  If you have brick sides and tops, you can continue to use the high suction.  You need to be careful around the elements so that you do not bump them.  This is where the brush attachment is most useful, as you can gently brush out any accumulated dust and any loose particles from the brick.

If you have fibre sides or top, the high suction setting on the vacuum will pull fibres from the refractory material.  You need to use a low setting to avoid damaging the insulating materials.  Gently pass the brush attachment along the insulating fibre and along the elements.

This vacuuming of the kiln does not need to be done on every firing, only at regular intervals.  It is also a good time to check the condition of the elements and condition of the interior of the kiln.  Any element tail connections can be checked for tightness.  The condition of the bricks can be checked as you vacuum. 

Of course, if you are going to fire an important piece, it is a good idea to make sure the kiln is clean before you start. But daily cleaning is not required.

It is not only the interior structure of the kiln that needs to be clean.  You should be checking the cleanliness of your kiln furniture too.  Make sure you keep the shelves dust free and regularly kiln wash them.  Check the kiln posts for flaking kiln wash and dust.  Clean off any dust or loose material and re-coat as necessary.  

And while you are doing all this cleaning, you could vacuum the outside of the kiln too.