Installing Leaded Glass in Stone

Side rebates
One side of the rebate (or raggle) in stone should be deeper than the other. This allows the panel to be slotted in and then slid back into the shallower rebate. Which side the deep rebate is on is not important, but you must determine which is the deeper and its minimum depth all along the raggle.

Adjusting the placement of the panel
To help move the panel from side to side stiff oyster knives and lead knives are important. This allows you to get behind the edge and slide the panel to the side, especially when it is sitting on top of another panel to make the fine adjustments to get the lead lines flow correctly.

In some circumstances, especially when installing a single panel, it is necessary to bend the leaves of the lead toward the installation side. After placing the panel, you then fold the leaves out one at a time into the raggle slot.

Top and bottom rebates
For the top and bottom rebates it is important that the top is the deep one. You insert the panel up into the slot a the top and let it settle into the bottom rebate. The panel should be completely covered by the stone.

Extra came
In all installations into stone, you should carry extra came of at least 12mm (1/2”) to solder round the panel when the stone work is not as accurate as it should be, either through workmanship or weathering.

Wedges
Have some little blocks of wood and some whittling tool to hand to wedge the panel in till mortared. It is possible to use little scraps of lead for the purpose. These wedges don't need to be that robust, they are just there to hold the panel in place until the mortar is in.

Mortars
Mortars for stone should be of lime cement, or sand mastic. Don't use silicon, you'll never get it out again! Also don't use putty as this stains some types of stone and the oils leech in to the stone, causing the putty to dry and therefore the window ceases to be watertight.

Brushes for Painting

A quality paint brush will have hairs that form a point and have a good spring to them - they bend while painting but return quickly to their original shape. A good brush will also hold lots of paint and deliver that paint evenly throughout the stroke. Brushes usually have a number to indicate their size - the larger the number, the larger the paintbrush. The larger the brush the wider the line that can be produced, although with a light touch a fine long line can be made because of the pointed nature of the brush.

The best brushes are made from natural hairs, although there are brushes made from a combination of natural and synthetic materials which are adequate.

Sable hair brushes are considered to be the best for painting. The hair comes from a variety of pine martin and the Kolinsky sable from Siberia is considered the best. These brushes are more expensive than others, but are soft and flexible, hold their paint well and can make an expressive thick to thin line.

Ox hairs are normally used for making rigger brushes. This is a round brush with long hairs, said to be used to paint the lines of ships' rigging in the past. The hair is strong and springy making it useful for long lines and thicker paints.

Squirrel hair brushes are useful for applying paint in broad, thin layers for matting.

Goat hair brushes are normally known as hake brushes. These are a traditional, oriental style brush. It lacks spring, but forms a good point and so is useful to cover larger areas quickly with a gentle touch.

Pony hair is made into short round brushes used as soft stipplers.

Hog hairs are made into hard, very economical brushes. They come in flat and round shapes. They are most used for stippling and can be trimmed, shaped, used, and abused for years.

Badger hairs are thicker at the end and thinner at the root, creating a conical shape. These soft brushes are used to blend paint once it has been spread on the glass. The brush is swept across the surface of the paint to blend or move paint and remove stroke lines.

Glass Shifting on Mould

There are a number of things to investigate if your blank is shifting on the mould during firing.

Is there a heat differential?

Glass absorbs heat at different rates depending on colour and type meaning that one part may begin to move before another. The solution to this is to slow down the rate of advance to allow all the glass to gain heat at the same speed. It may also be useful to slump at a lower temperature.

There also may be a heat differential within the kiln. You need to run a check on the heat distribution of your kiln to be sure where the (relatively) hot and cold areas of your kiln are. Bullseye published Tech Note no.1 on how to do this.

Not perfectly balanced on the mould?

Glass can be placed just off square or level and that can allow it to start slumping unevenly. Measurements and observation can help to get the glass placed squarely on the mould. Also a small spirit level placed on the glass can tell you if the glass is level within the mould.

The mould may not be level.

The kiln, shelf and mould should each be checked for level in all directions. The kiln level can be established and can be assumed to be level until it is moved. The shelf level should be checked each time it is moved. The mould level should be checked each time it is used.

Is the glass overhanging the mould?

Glass overhanging the mould rim can hang up on some of the edges more than others. Check the rim of the mould for any rough areas and smooth them. If you do have glass overhanging, you should slow the rate of advance to allow the edge of the glass to tip up and begin to slide down into the mould. If the problem persists, make the glass blank smaller, or support the overhanging glass with a collar.

Is the glass heavier on one side?

The glass may be uneven thickness and so heavier on one side. The heavier area of the glass will begin to slump first and so promote movement of the whole glass in an asymmetrical manner. The solution to this is to fire slower and to a lower temperature.

Do you have a wonky mould?

The mould can be imperfect. So you need to check the mould for accuracy. I have a slumper that has one side lower than the other three. Being aware of this, I can place the glass so that it is still useable. Measuring the mould in all directions will help determine its symmetry.

If all these things have been investigated and the solution not found, it is possible to create a bevel on the bottom edge of the glass so that the edge sits in the mould at the same angle as the mould. This provides a larger contact point for the glass and mould than just a thin edge. This appears to allow the glass to move evenly during the slump.

Of course, a major solution is to observe the slump.  Peeking into the kiln at the beginning of the slump soak and frequent intervals after that will show if the piece is slumping evenly or not.  If it is uneven, you can put on the appropriate protective gear and with gloves on your hands, shift the glass to be set evenly in the mould.

The major solutions to avoid uneven slumping are:

• Avoiding the hot and cool parts of the kiln
• Making everything level
• Careful placement on the mould
• Slower rates of advance
• Lower slumping temperatures
• Observation

Using Space on Shelves

Often there is unused space on the kiln shelves when you are firing a project. With a bit of planning, you can make use of the spaces for a variety of things.

Frits fired on fibre paper

Bowl made from frit balls

You can place piece of frit in the clear areas to make frit balls.

You can make colour tests on plaques of glass to see the results of strikers, powder combinations or results of various depths of colour.

Compatibility tests can be done with pieces of glass of which you are not certain.

simple stress testing set-up

Strip of fired glass samples for testing

Results - those with halo are stressed

In the same way, annealing tests can be conducted.

You can fire small pieces of jewellery at the same time as your larger pieces.

You can also prepare elements for incorporation into other fusing projects and lay them out in the open spaces on the shelf.  Your use of the spare space is related both to your imagination and to your future projects.

Cleaning Blending Brushes

Cleaning badger brushes just before use, is easy. Flick, gently and rapidly, the very ends of the brush hairs against the side of your hand – but use respiratory protection and be careful not to inhale any dust. If you notice flecks of dust in your paint when you create a grisaille you’ll know it’s time for a thorough and wet cleaning again.

After each use, rinse out the brush tips in cool water. Gently rub the tips of the brush hairs to loosen any extra paint. Grasp he hairs above the tips to keep the water from the main part of the brush. Then wet the exposed ends of the hairs and rub them gently until the water runs clear. 

If you use a blender for oil, you will need to use a small amount of natural soap, if so, thoroughly rinse.

Flick the brush to remove excess water, smooth the hairs into shape and allow to completely dry by hanging the brush with the hairs pointing downward – this avoids water flowing into the brush base where the hairs are attached. If you have round-handled brushes, you can twirl the brush between your hands to remove excess water.

Shape of Aperture Drops

The shape of an aperture drop can be controlled by the speed of the slump. The speed at which the glass drops is a combination of heat and size of the hole. Patience is required.

Rapid drops result from high temperatures. Rapid slumps cause a thinning of the glass at the shoulder where the glass turns over the inner rim of the aperture. The pattern is distorted and the colours are also diluted. And a relatively large rim is left around the fired piece.

A much slower rate of drop spreads the strain of the slump over the whole of the unsupported area of glass. This tends toward a bowl with a gentle slope toward the bottom, reduced distortion of the pattern, maintenance of the colour densities, and a more even wall thickness all over the piece.

The slumping temperature for a shallow angled slump is less than that used for normal slumps, and takes a lot longer – up to five hours typically. This means that observation is required at intervals, say every half hour.

A starting point for the slumping is around 100ºC above the annealing temperature for the glass. So for Bullseye and System 96 the temperature is about 615ºC. If after the first half hour, there is no movement, increase the temperature by 10ºC. Check again in another half hour and if the slump has begun, leave the temperature at that level and observe at the half hourly intervals until the desired slump is achieved. Otherwise, increase the temperature by another 10ºC with the check after half an hour, and repeat until the slump has begun. After you have done the first one of these with a particular size of aperture, you will know the temperature to start the slump.

The temperature you need to use is affected by the size of the hole. The smaller the aperture, the higher the temperature will be needed. But be patient. If the temperature is increased too much, you will get the thinning of the sides that you are trying to avoid.

Additional information on aperture drops can be found in this series.

Lead Came with Alloys

Lead came is available in several hardnesses. One (soft) is almost pure lead, another is half hard and contains up to 5% antimony, and the third is hard, containing up to 10% antimony. The difference between these is hardness, or resistance to creep, not resistance to corrosion.

elemental lead

Lead with antimony as an alloy is subject to the same corrosion rate in atmospheric environments as chemical lead (99.9% commercial-purity lead). However the greater hardness, strength and resistance to creep of antimonial lead often makes it more desirable for use in specific chemical and architectural applications.

The ability of some antimonal leads to retain this greater mechanical strength in atmospheric environments has been demonstrated in exposure tests in which sheets containing 4% Sb [antimony] and smaller amounts of arsenic and tin were placed in semi-restricted positions for 3 years. They showed less tendency to buckle than chemical lead, indicating that their greater resistance to creep had been retained.

Handbook of Corrosion Data, by Bruce D Craig, p89ff

Antimony crystals

Thus, the use of softer leads in conservation or restoration, because they were used in earlier periods, is not indicated. It is known that lead came up to sometime in the early 19th century was melted and re-formed into came, incorporating tin from solder and other trace elements which made the lead “stiffer” than the more pure lead that began to be produced commercially and used widely at that time. This may be the reason that so many 19^th century windows contain failing leads, while many earlier ones remain sound.

Pink Confetti

Because confetti needs to be so heavily saturated with colour, some of the opalescent colours tend to devitrify. The pink is particularly prone to devitrification. There are several ways to prevent this: 

• cap (which can lead to bubbles), 
• add a devitrification spray, or 
• cover with clear powder or frit.

Covering completely with a fine layer of powder gives the most even result. Using frit can provide a speckled appearance that is useful in some circumstances.

This tendency of pink opal to devitrification applies to all formulations – Bullseye, Uroboros, S96 and float.

What is Viscosity

What is Viscosity?

An example of differing viscosities

There are a variety of definitions, but these two capture the main elements.

Informally, viscosity is the quantity that describes a fluid's resistance to flow. Fluids resist the relative motion of immersed objects through them as well as to the motion of layers with differing velocities within them.  Source

Viscosity is a measure of a fluid's resistance to flow. It describes the internal friction of a moving fluid. A fluid with large viscosity resists motion because its molecular makeup gives it a lot of internal friction. A fluid with low viscosity flows easily because its molecular makeup results in very little friction when it is in motion.  Source

A demonstration of the resistance of different viscosities of oil to a weight moving through the liquid.

Almost all liquids are viscous fluids having viscidity. For example, when rotating a drum container filled with water on its vertical central axis, the water that was at rest in the beginning starts moving as it is dragged by the container’s inside wall and then whirls completely together with the container as if it were a single rigid body. This is caused by the force (resistance) generated in the direction of the flow (movement) on the surfaces of the water and the container’s inside wall. A fluid that generates this kind of force is regarded as having viscosity.

Temperature is a very important factor for measuring viscosity. In fluids, as temperature goes up, viscosity goes down and vice versa. In the case of distilled water, if the temperature changes 1 centigrade, it produces a difference of 2 % to 3 % in viscosity.  Source

Viscosity is the measurement of a fluid's internal resistance to flow. This is typically designated in units of centipoise or poise but can be expressed in other acceptable measurements as well. Source

Why is viscosity important?

“Near the strain point the expansion increases rapidly and sometimes erratically.” The links between the molecules has reduced in strength and so have a lesser role in the forces acting at higher temperatures. “In those upper ranges – the temperatures where glasses are formed and re-formed with heat – viscosity is a much more useful indicator of how glasses will behave.

“The combination of viscosity and COE are what make glasses more or less compatible, i.e., containing stress in amounts low enough to allow them to hold together without breaking at room temperature for extended periods of time under normal circumstances.

Bullseye found in the early 1980s in their efforts to mix coloured glasses in streaky colour combinations that the COE could not be used to predict compatibility. In trying to correct the compatibility of certain mixed glasses, the closer they brought together the COEs, the more incompatible became the mixes.

“The reason that we could not use COE to successfully predict whether a coloured glass would fit the base clear glass was/is because, as the base glass composition is altered with the addition of the necessary oxides to colour it, the viscosity is inevitably changed. This viscosity change causes the coloured glass and the clear base glass to strain themselves in the cooling cycle of the fusing process (a viscosity mismatch). Therefore once the two glasses reach room temperature they have undue residual strain that may lead to failure.

“In order to prevent this undue residual strain an equal but opposite strain must be introduced into the coloured glass to cancel out the strain induced by the viscosity mismatch. This is accomplished by introducing an expansion mismatch of equal but opposite strain. The two mismatches cancel each other out, leaving the two glasses nearly strain free.

“It is this phenomenon (viscosity mismatch cancelled out by an equal but opposite expansion mismatch) that enables glasses of very different compositions to be formulated to fit each other. The very fact that the expansion of a coloured glass has to be altered to make it fit a base clear glass implies that COE cannot be used as an indicator of compatibility. It is also why it only makes sense to describe these glasses as tested compatible to a specific manufacturer's base glass for a specific glass forming process.“ [L. MacGreggor]

Even different formulations of glass have different viscosities and different rates of softening with temperature increases.

How does viscosity apply to us?

Although viscosity is of major importance to the manufacturer, it does have some relevance to kiln formers too.

Understanding that glasses have different viscosities – most often referred to as hard and soft – can help in the choice of colours and styles of glass to combine. Some glass will spread more, and also allow other glass to sink deeper into the layer than others. It might help avoid combining extremely hard and soft glasses next to each other.

It should also help explain some results that were not planned. It may help in when thinking about uneven slumps.

It is important to recognise that glass chemistry is extremely complicated, and to see that the expansion characteristics have to be balanced with the viscosity characteristics as the two main elements in compatibility. There are others, of course, but these appear to the two main ones.

Bubble Reduction in Casting

There are several things that can be done to reduce the number and size of bubbles in casting.

• Fire higher - to 830ºC instead of 815ºC - and soak for at least four hours. This allows more bubbles to rise to the top and burst. If there are still more bubbles than wanted, increase the soak time.

• Stack the glass in the centre of the mould, allowing a few centimetres from the mould walls. This allows the glass to spread and flow from the bottom and up the sides, reducing the likelihood of trapping air. If you have more than one stack, keep the same space between the stacks as the mould walls.

• Make sure that the way you stack the billets or casting plates so there is a smaller space at the bottom of any cavity than at the top. The reverse allows the glass to soften and seal in the air in the space.

• You can construct a mould to make billets of the general shape of the final object. This of course, is much more work, needing two moulds.

• A major thing to avoid is the use of frit, especially at the bottom or deep in the mould as bubbles will collect around each piece and lead to a multiplicity of bubbles throughout the casting.