Wednesday, 6 March 2024

Slumping Strategy

A schedule was presented for a slumping problem of a 6mm/0.25” blank.  It consisted of three segments each of a rate of 277C/500F with short holds up to 399C/750F and then a rapid rise to 745C/1375F.  The cool was done with two long holds at 537C/1000F and 482C/900F followed by cooling rates for 12mm/0.5”



My response was that, yes it was fired too high.  Not only that, but the firing strategy, as shown by the schedule, is odd. 

Strategy

The general strategy for slumping follows these ideas.

·        Glass is slow to absorb heat, and in one sense, this schedule accepts that by having short soaks at intervals.  As glass is slow to absorb heat, it is necessary to use slow ramp rates and without pauses and changes in rates.  This should be applied all the way to the slumping temperature.

·        Holds of short durations are not effective at any stage in a slumping firing.  The objective is to allow the glass time to form to the mould with as little marking as possible.  This implies slow rates to low temperatures with significant holds at appropriate stages.  This about putting enough heat work into the glass that higher temperatures are not needed.

·        This kind of firing requires observation for new moulds and new arrangements of glass to ensure the slump is complete.  Once you know the mould requirements and are repeating the layup of the glass, the firing records will tell you what rates and times to use to get a complete slump with minimum marking.

·        The hold at annealing temperature is to equalise the temperature throughout the glass to produce a stress-free result.  Any soaks above are negated or repeated by the necessary soak at the annealing temperature.  The hold there must be long enough to complete the temperature equalisation that is the annealing.

·        My work has shown that annealing for one (3mm/0.125”) layer thicker produces a piece with less stress.  This indicates that a 6mm/0.25” piece should be annealed as for 9mm/0.35” to get the best result.

The summary of the firing strategy for slumping is:

  • ·        A single ramp of a slow rate to the slumping temperature.
  • ·        Observation of the progress of the slump to determine the lowest practical temperature and hold time.
  • ·        Annealing for one layer thicker that being slumped.
  • ·        Three stage cooling of the piece at rates related to the annealing hold.

Critique

This is a critique of the schedule. For comparison, my schedule for a full fused 6mm blank would be different.

  • ·        140ºC/250ºF to 677º/1250ºF for 30 to 45 minutes.
  • ·        9999 to 482ºC/900ºF for 1.5 hours
  • ·        69ºC/124ºF to 427ºC/800ºF, no hold
  • ·        125ºC/225ºF to 371ºC/700ºF, no hold
  • ·        330ºC/600ºF to room temperature, off.

The rate of the published schedule is fast for a full fused blank and extremely fast for a tack fused blank. This needs to be slowed.  The schedule provides a single (fast) rate of heating, but with unnecessary holds.  The holds are so short as to be ineffective, anyway. There is no need for the holds on the way up to the slumping temperature.  In general slumping schedules are of fewer segments.   This is because glass behaves well with steady slow inputs of heat.

Then strangely, the schedule increases the rate to top temperature.  It does so with a brief soak at 593ºC/1100ºF.  This fast rate of 333ºC/ 600ºF begins at 400ºC/750ºF.  This is still in the brittle phase of the glass and risks breaking the glass.  The brittle stage ends around 540ºC/ 1005ºF.

This rapid rate softens the surface and edges of the glass without allowing time for the underside to catch up.  This explains uneven edges.  It also risks breaking the glass from too great expansion of the top before the bottom.

Additionally, the schedule uses a temperature more than 55ºC/100ºF above what is a reasonable highest slumping temperature.  The top temperature of this schedule is in the tack fusing range.

There is no need for a hold 55ºC/100ºF above annealing soak. It is the annealing soak that equalises the temperature before the cool begins.  The higher temperature equalisation is negated by the cooler soak at annealing temperature. So, the hold at the higher temperature and slow cool to the annealing temperature only delays the firing by about two hours.  It does not have any effect on the final piece.

The schedule is cooling for a piece of 12mm/0.5”.  This is slower than necessary.  As noted above, cooling for one layer thicker than the piece is advisable to get the most stress free result.  The annealing soak could be 1.5 hours following this idea.  Cooling with a three stage schedule reduces the risk of inducing temporary stresses that might break the glass.  Although the initial cooling rate I recommend is very similar to this schedule, it safely reduces the total cooling time.

  • ·        69ºC/124ºF to 427ºC/800ºF, no hold
  • ·        125ºC/225ºF to 371ºC/700ºF, no hold
  • ·        330ºC/600ºF to room temperature, off.

Using my kind of schedule for the first time will require peeking once top temperature is reached to determine when the slump is complete. It may take as much as an hour. Be prepared to either extend the hold, or to skip to the next segment if complete earlier. The controller manual will explain how.

 More information is given in Low Temperature Kilnforming, An Evidence-based guide to scheduling.  Available from Etsy and Bullseye


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