Drying kiln wash

“Dry your kiln wash between coats and before firing.” 

This is a frequent statement when talking about renewing kiln wash on shelves and moulds.  The main reason given seems to be that there will be less risk of creating bubbles by evaporating moisture.  The air drying will reduce moisture in kiln is a second reason.

There are some difficulties with this statement and reasons.

Drying between coats of kiln wash means you are applying liquid over powder. This can promote clumping and streaking through a too rapid absorption of water by the dry kiln wash. Also, it makes applying kiln wash a lengthy process.  It is not like painting a door or even a floor, where you must allow drying to avoid streaks. 

Credit: Ceramicartsnetwork.org

Applying kiln wash by brushing is smoothest if all coats are done at once.  This is what happens if you spray kiln wash on your shelves and that gives a smooth surface.  If it were otherwise, drying between coats would apply to spraying too.  Drying between coats promotes streaks in the applied kiln wash that needs to be smoothed before use.  This of course, does need to be done after the kiln wash has dried.

Drying before using the shelf or mould is unnecessary. The evidence I have to offer is that I frequently fire within an hour of applying fresh kiln wash to a cleaned shelf. I have had no problems with creating bubbles or glass picking up the kiln wash. The shelf dries, with a moderate rate of advance, long before the glass settles into the texture of the surface.  It is only as the glass settles into the contours of the kiln wash that it seals air, or any other material, under the glass.

The pigment in most kiln washes is to tell you which shelves have not yet been used.  If they are fired dry at even moderate temperatures, the pigment disappears.  Then you have removed that indicator of freshly prepared shelves or moulds.

Drying of kiln wash before use in not necessary.  If you wish to be cautious, air drying will be enough to avoid any problems with moisture.

What are enamels?

Not all enamels are equal

Enamel paints

This description refers to a paint that air dries (or with minimal heat) to a hard finish (usually gloss). Most commercially available enamel paints are significantly softer than either vitreous enamel or heat cured synthetic resins. The term "enamel paint" generally is used to describe oil-based covering products, usually with a significant gloss finish. Many latex or water-based paints have adopted the term.

Enamel paint has come to mean a "hard surfaced paint" and usually is in reference to paint brands of higher quality, floor coatings of a high gloss finish. Most enamel paints are alkyd resin based. Some enamel paints have been made by adding varnish to oil-based paint. Enamels paint can also refer to nitro-cellulose based paints. Nitro-cellulose enamels are also commonly known as modern lacquers.  These have been largely replaced by synthetic coatings like alkyd, acrylic and vinyl.

More information at: https://en.wikipedia.org/wiki/Enamel_paint

Enamel paints are used for coating surfaces that are outdoors or otherwise subject to hard wear, or variations in temperature.  A widespread application is in paints for cars. It is also used frequently to decorate or label bottles due to the low curing temperatures of some formulations.

Vitreous enamels 

Vitreous enamels are used in a variety of circumstances.  Metal signs are most frequently enamel coated; they are used in ceramics as over glazes;  and they are used on glass in many circumstances.

Vitreous Enamel is simply a thin layer of glass fused at high temperature on to the surface of a metal or glass. Vitreous Enamel can be defined as a material which is a vitreous solid obtained by smelting or fritting a mixture of inorganic materials.  The word enamel comes from the High German word ‘smelzan’ and from the Old French ‘esmail’.

The key ingredient of vitreous enamel is finely ground glass frit. Colour in enamel is obtained by the addition of various minerals and metal oxides. 

Vitreous enamel is made by smelting naturally occurring minerals, such as sand, feldspar, borax, soda ash, and sodium fluoride at temperatures between 1200°C and 1350°C  until all the raw materials have dissolved. The molten glass which is formed is either quenched into water or through water-cooled rollers. This rapid cooling prevents crystallisation. The resulting frit is ground in a rotating ball mill either to produce a water-based slurry or a powder.

At the milling stage, other minerals are added to give the properties and colour required of the final enamel. Different enamel colours can be mixed to make a new colour, in the manner of paint. Enamel can be transparent, opaque or opalescent.

More information at: 

https://www.vea.org.uk/what-is-enamel/

https://en.wikipedia.org/wiki/Vitreous_enamel

https://www.iom3.org/vitreous-enamellers-society/vitreous-enamel-information

Metal enamelling

Modern frit for enamelling steel is typically an alkali borosilicate glass with a thermal expansion and glass temperature suitable for coating steel and other metals. Raw materials are smelted together between 1,150 and 1,450°C (2,100 and 2,650°F) into a liquid glass that is directed out of the furnace and thermal shocked with either water or steel rollers into frit. Vitreous enamel is often applied as a powder or paste and then fired at high temperature. This process gives vitreous enamel its unique combination of properties. The smooth glass-like surface is hard; it is scratch, chemical and fire resistant. It is easy to clean and hygienic.  It all started 3500 years ago in Cyprus. Since 1500 BC, enamelling has been a durable, attractive and reliable material.

More information at: 

https://en.wikipedia.org/wiki/Vitreous_enamel

https://www.vea.org.uk/what-is-enamel/ 

Enamels in Ceramics

Overglaze decoration, overglaze enamelling or on-glaze decoration are all names for the method of decorating pottery, where the coloured decoration is applied on top of the already fired and glazed surface, and then fixed in a second firing at a relatively low temperature.  The colours fuse on to the glaze, so the decoration becomes durable. This decorative firing is usually done at a lower temperature which allows for a varied and vivid palette of colours, using pigments which will not colour correctly at the high temperature necessary to fire the clay body.

More information at:  https://en.wikipedia.org/wiki/Overglaze_decoration

Glass Enamels

Glass enamels are produced in the same way as enamels for metals and ceramics.  The frit characteristics are adjusted for various applications and temperatures.  This combination of finely ground frit and metals for colouring are often combined with a binder or carrier medium.  It is similar to vitreous enamel on metal surfaces, but the supporting surface is glass. It is also close to "enamelled" overglaze decoration on pottery, especially on porcelain, and it is thought likely that the technique passed from metal to glass (probably in the Islamic world), and then in the Renaissance from glass to pottery (perhaps in Bohemia or Germany). 

Glass may be enamelled by sprinkling a loose powder on a flat surface, painting or printing a slurry, or painting or stamping a binder and then sprinkling it with powder, which will adhere.  The powdered frit can be in the ceramic on-glaze composition suitable for fusing or casting temperatures, or it can be adjusted for slumping temperatures as in the traditional glass stainers’ enamels. It can produce brilliant and long-lasting colours, and be transparent, translucent or opaque. Generally, the desired colours only appear when the piece is fired, adding to the artist's difficulties.

More information at:  https://en.wikipedia.org/wiki/Enamelled_glass

The term enamel is applied to a wide variety of coating materials.  The range of usage is indicated, and the manufacture and applications of vitreous enamels is indicated.  The term enamel is not properly applied to finely ground coloured glass in a medium.

Materials for making dams

Rectangular or straight sided shapes

Broken shelves

Accidents happen to mullite shelves causing breaks or cracks.  Rather than throwing them out, you can cut them into rectangles or 50mm strips with a tile saw.  The resulting shapes need to be kiln washed to keep glass from sticking.  They can be used flat or stood on their edges with supports on the outside.

Thick ceramic tiles can be used in much the same way.  You do need to remove the glaze from the tile to make sure they don’t stick to the glass.  Or you could use the unglazed side toward the glass. Again, the tiles need to be kiln washed.

Stainless steel can be used as a dam.  It will need treatment with a separator such as boron nitride or kiln wash.  In addition, it needs to be lined with refractory fibre paper to cushion the force of the greater contraction of steel than glass.

These materials cannot easily be adjusted in length to fit the size of the glass piece being dammed.  Instead, arrange them in a swastika like formation. 

This photo also shows how shorter lengths can be incorporated to make the whole dam.

Vermiculite board is a refractory material that can be used to form dams by cutting with a wood working saw.  The saw you use to cut the vermiculite will be dulled and only be useful for cutting vermiculite in the future.  Do not use any expensive cutting equipment!  

Credit: Bullseye Glass Company

Refractory fibre board is available in many thicknesses.  It can be cut with craft knives even though it dulls the blades quickly.  The thicker boards can be used without rigidising.  This avoids the need to kiln wash and allows adjustments in length.  If you do rigidise fibre board, you must coat it with a separator such as kiln wash or boron nitride.

Weighted fibre paper can be used.  It is sometimes the quickest and easiest to use, as there normally is a stash of scraps around the studio.  It is easily cut with a craft knife.  You can build up the thickness of the dam by layering pieces on top of one another.  Sometimes people put metal wire or pins in the layers to ensure there is no movement between the layers. I’ve found that if weighted, the fibres interlock enough that the layers do not shift.  But you need to line the layered fibre paper dams with vertical strips of fibre paper, so the glass does not take up the layered dam profile on its edge.

Note that you need to use breathing protection when cutting all these materials.

Curved and circular pieces

Many times, the shape to be dammed is not formed of straight lines.  Different materials need to be used in these cases.

Formed stainless steel is a good durable and reusable material.  You need to line the shape with fibre paper if it completely contains the shape, because it contracts more than the glass and can crush the piece.  It is expensive to have made and so needs to have multiple uses to justify the cost.  A cheaper alternative is to make your own shape using stainless steel strapping as used for shipping crates and pallets. 

Fibre paper is an excellent material for damming irregular shapes.  It can be cut into complicated shapes, and it can be layered to attain the required height. You can weight it if you are taking things to a high temperature and fear that the glass will flow under the fibre paper.

You can also use the thicker fibre papers upright by backing up with multiple pieces of kiln furniture to maintain the shape you desire.

Vermiculite board is a good material for making shapes, although not as complicated ones as possible in fibre paper.  Vermiculite can be shaped with wood working materials, but cheap ones should be used as they are quickly dulled. You can rough out a shape with a jigsaw and refine it with various wood working tools, including coarse sandpaper.  Because it is a relatively rigid material, a lot of inventiveness can be used in forming the edges by altering angles from the vertical, incising designs into the edge, etc.  Be certain that you have adequately kiln washed or put other separator on the board, as it will stick to the glass if left bare.

Fibre board is a less rigid material than vermiculite, but is easier to work with simple craft tools.  It is simple to use for a unique one-off shape. It only needs smoothing and does not have to have a separator applied because it does not stick to the glass.  If you create a shape that you will want re-use, you can rigidise the board after shaping, but it will require separators then.

Note that when working with refractory materials, you need to wear respiratory protection and clean surfaces with a HEPA vacuum or by dampening dusty surfaces and wiping them clean.  Dispose of cleaning materials safely.

Colour Dilution of Powders

Sometimes you do not have a tone or shade of a colour you need for your project.  Other times you want to have a gradation of shade across a piece.  There is the obvious solution of mixing a colour with clear to produce lighter shades.  But there is a difficulty when mixing clear with powders to fuse. The result is often a pointillist effect with points of light coming through the colour. There are several approaches to this difficulty.

One way is to use a powder made from a tint of the colour.  But sometimes there is not a tint made. Sometimes you do not have that tint in stock. So, you must look to other solutions.

Credit: www.warm-glass.co.uk

An alternative is to use clear powder to mix with the intense colour you want to dilute.  You will need to test varying proportions of clear to colour to get the tone you need.  You may be surprised at the amount of clear needed.  And there still is the slight possibility of points of light coming through the clear.

Another possibility is to use one of the less dense white powders to mix with the colour.  White powders such as the Bullseye 000243, translucent white, or the 000113, dense white are possible.  The very dense or lacy whites are not as suitable. One is too opaque, the other is uneven in colour. Again, testing will be required, and you may be surprised at how little is required to alter the tone.

One other way I have used is to mix fine frit with the powder.  This has less control than the other methods but can provide significant dilution of the intense colours.  If you want to see if this is suitable, you can follow this process. 

Add a few drops of water to the clear frit in a small container. Close it and shake to get all the frit coated with a film of water. If after shaking the frit is not “clumping” you can add a little more. Too much water will create a slurry which is not suitable.  So, add only a small amount of water at a time until the frit is like damp sand on the beach. Any excess water must be poured off. 

Add powder to the damp frit, and shake well again to coat the frit with powder. If the frit does not seem to be fully coated, add a little more powder.  The film of water on the frit allows the powder to adhere temporarily to the frit.  

This mixture can then be applied to the surface and smoothed with a pallet knife. This will not guarantee there are no clear pinpoints, but it will reduce them to a minimum. You will not have the subtle differences in tone that sifting powder can give you, but it is a cost-effective way of diluting intense powder colours that can have advantages over mixing powders.

Of course, the various methods of diluting colour described here can be used to combine powders to produce new colours.

Sharp points on rectangles

At the conclusion of firing pieces with right angles or sharper shapes you often find very sharp needle points at the corners.

This is a result of the expansion of the glass as it heats up.  At top temperature, the glass piece is larger on the shelf than when you put it in cold.  The amount of this expansion is related to the thickness of the piece and the temperature it has been fired at.

As the glass cools, it contracts.  The contraction at corners and points has greater effects on the glass than at the sides.  The corners are contracting from two sides rather than only one.  This makes them a little more resistant to contract and often leaves a little of the glass stuck at the furthermost point of expansion as it contracts.

I have found the best prevention of sharp points on the corners of rectangular pieces, and those with even sharper angles, is to nip off the tiniest bit of the corners. This very slight blunting of the corners allows the glass to expand and then retract without the corner or point catching on the separator and so creating the sharp needles.

Further information is available in the e-book: Low Temperature Kilnforming.

Soaks Below the Softening Point

There are frequent suggestions that holds in the rise of temperature for glass are required.  Various justifications are given.  A few notes before getting to the explanation of why they are uncessary.

A note is required about the softening point sometimes called the upper strain point. There is a reasonable amount of discussion about the lower strain point.  So much that it is often simply referred to as the strain point.    Below the lower strain point, the glass becomes so stiff and brittle that no further annealing can occur.  Thermal shock can happen though, so the cooling needs to be controlled.

There also is an upper point at which the behaviour of the glass is different.  Above this temperature, no annealing can occur either, because the glass has become plastic and the molecules randomly arranged.  It is only just pliable, of course, but its molecules are no longer strongly bound to one another.  This is the temperature at which much of slumping is done.

It is disputed whether such a point exists.  Still, in practical terms it is where the glass becomes so plastic that it cannot be temperature shocked.  The temperature of this “point” is approximately 45°C above the annealing point, rather than the temperature equalisation soak. 

Note that the temperature at which Bullseye recommends that the annealing soak should occur is a temperature equalisation point, which is about 33°C below the glass transition temperature - the point at which glass can be most quickly annealed.  The average glass transition point for Bullseye is 516°C.  Most other fusing glasses use the glass transition (Tg) point as the annealing temperature for the soak.  They or you could employ the Bullseye technique on thicker slabs of the glass by setting the temperature equalisation point 33°C below the annealing point, and soaking for the same kinds of time used in the Bullseye chart for annealing thick slabs.  In fact, this is what Wissmach has recently done with its W90 and W96 fusing glass ranges.  They now recommend 482C (900F) as the anneal soak temperature.

Now to the point of the post.

The soaks that are often put into schedules on the rise in temperature are justified as allowing the glass to equalise in temperature.  Glass in its brittle phase is an excellent insulator.  This means that heat does not travel quickly through the glass.  Consequently glass behaves best with steady and even rises in temperature (and correspondingly on the reduction in temperature).  Rapid rates risk breaking the glass on the temperature rise, no matter how many or how long the holds are.  

This means a slower rate of advance will accomplish the heating of the glass in the same amount of time, and in a safer manner, than rapid rises with short soaks/dwells/holds.  The slower rate of temperature increase allows the glass to absorb and distribute the heat more evenly.  This slow heating is most obviously required in tack fusing where there are different thicknesses of glass.  

This means that it is possible for thin areas of glass to heat up much more quickly than glass covered by different thicknesses of glass.  It also applies to strongly contrasting colours such as black and white, because they absorb the heat differently - black more quickly than white.

There are, of course, circumstances where soaks at intervals are required – usually because of mould characteristics, in slumping, and in pate de verre.

Sometimes people add a soak at the annealing temperature on the way up in their schedules.  This is unnecessary.  If the glass has survived up to this point without breaking, it is highly unlikely it will break with a further increase in the rate of advance unless it is very fast.  The temperature after all, is above the strain point meaning the glass is no longer in the brittle phase.

Many people add a soak at around 540°C (ca. 1000°F) into their schedule on the increase in temperature, before their rapid rate of advance to the top temperature.  The choice of this temperature relates to the lower strain point.  This also is unnecessary, except possibly for very thick pieces. By this time the glass has reached its plastic stage and if it hasn’t broken by then, it won’t with a rapid rise in temperature either.

Further information is available in the ebook Low Temperature Kiln Forming.

Soaks at various temperatures during the advance to the upper strain points of glass are not necessary.  What is necessary is a knowledge of when the glass becomes plastic in its behaviour, and an understanding of how soaks can overcome characteristics of moulds, or how to achieve specific results and appearances of the glass.

Effects of Dams on Scheduling

 I recently made a statement about the effects of various dam materials on the scheduling.  This was based on my understanding of the density of three common refractory materials used in kilnforming – ceramic shelves, vermiculite board and fibre board.  I decided to test these statements.  I found I was wrong.

I set up a test of the heat gain and loss of the three materials.  This was done without any glass involved to eliminate the influence of the glass on the behaviour of the dams.  The dam materials were laid on the kiln shelf with thermocouples between.  These were connected to a data logger to record the temperatures.

 

The schedule used was a slightly modified one for 6mm:

300°C/hr to 800°C for 10 minutes

Full to 482°C for 60 minutes

83°C to 427, no soak

150°C to 370°C, no soak

400°C to 100°C, end

 

The data retrieved from the data recording is shown by the following graphs.

 

Highlights:

·        The dam materials all perform similarly. 

·        This graph shows the dams have significant differences from the air temperature – up to 190°C – during the first ramp of 300°C/hr. (in this case). 

·        There is the curious fall in the dams’ temperatures during the anneal soak.  This was replicated in additional tests.  I do not currently know the reasons for this.

·        The dams remain cooler than the air temperature until midway during the second cool when (in this kiln) the natural cooling rate takes over.

·        From the second cool to the finish, the dams remain hotter than the air temperature.

 

Some more information is given by looking at the temperature differentials (ΔT) between the materials and the air.  This graph is to assist in investigating how significantly different the materials are. 

This graph is initially confusing as positive numbers indicate the temperature is cooler than the material being compared and hotter with negative numbers.

 

As an assistance to relating the ΔT to the air temperature some relevant data points are given.  The data points relate to the numbers running along the bottom of the graph.

Data Point   Event

    1                Start of anneal soak.

    30              Start of 1^st cool (482°C)

    45              Start of 2^nd cool (427°C)

    65              Start of final cool (370°C)

    89              1^st 55°C of final cool (315°C)

    306             100°C

 

At the data points:

·        At the start of anneal soak the ΔT between the dams is 16°C with the ceramic shelf temperature being 18°C hotter than the air.

·        At the end of the anneal soak of an hour, the air temperature is 20°C higher, although the ΔT between the dams has reduced to 12°C.

·        At the end of the 1^st cool the ΔT between the dams has reduced to 9°C and the ΔT with the air is 3°C.

·        At approximately 450°C the air temperature becomes less than the dams. 

·        At 370°C the hottest dams are approximately 17°C hotter than the air.  The ΔT between the dams is 10°C.

 

More generally:

·        The air temperature tends to be between 17°C hotter and 17°C cooler than the ceramic dams during the anneal soak and cool.  The difference gradually decreases to around 8°C at about 120°C.

·        Ceramic and fibre dams loose heat after annealing at similar rates – generally having a ΔT between 4°C and 1°C, with a peak difference of 9°C at the start of the second cool. This means the heat retention characteristics of ceramic strips and fibre board are very close.

·        Between the annealing soak and about 300°C the vermiculite is between 12°C and 9°C hotter than the same thickness of fibre.  Vermiculite both gains and loses heat more slowly than the ceramic or fibre dams do.  This means that vermiculite is the most heat retentive of the three materials.

Conclusions

·        Dams will have little effect during the heat up of open face dammed glass.  The slight difference will be at the interface of the glass and the dams where there will be a slight cooling effect on the glass.  Therefore, a slightly longer top soak or a slightly higher top temperature may be useful.

·        The continued fall in the dams’ temperature during the anneal soak indicates that this soak should be extended to ensure heat is not being drained from the glass by the dams to give unequal temperatures across the glass with the risk of inadequate annealing.  I suggest the soak should be extended to that for glass of 6mm thicker than actual to account for this.

·        The ability of ceramic and fibre dams to absorb and dissipate heat more quickly indicates that they are better materials for dams than vermiculite board.  The slightly better retention of heat at the annealing soak, indicates that ceramic is a good choice when annealing is critical.

Scheduling Effects 

Based on these observations, I have come to some conclusions about the effect of dams on scheduling.

·        There is no significant effect caused by dams during the heat up, so scheduling of the heat up can be as for the thickness of the glass.

·        The lag in temperature rise by the dams indicates a slightly longer soak at the top temperature (with a minor risk of devitrification), or a higher temperature of, say 10°C can be used.

·        The (strange) continued cooling of the dams during the annealing soak indicates that extending the soak time to that for a piece 6mm thicker than actual is advisable.

·        The cool rates can continue to be as for the actual thickness, as the dam temperatures follow the air temperature with little deviation below the end of the first cool. 

·        Ceramic dams perform the best of the three tested materials.

 

Smooth Surfaces on Drop Vessels

It is widely recognised that the usual results of kiln forming are one textured side and a smooth upper side. The common methods of having upper and lower surfaces both smooth is to blow the glass, avoid allowing the glass to touch the mould, and cold working the textured side to smooth.

The question arises about the possibility of getting smooth surfaces on the inside and outside of a drop vessel.  As the glass in a drop only touches the mould at the collar and edge, shouldn’t the glass be smooth on both sides?  The answer to that is in the temperatures and time used.

The temperatures used in a drop are not high enough to be certain of smoothing the outer surface.  But the soak times at drop temperatures are enough to create a fire polish on the upper/inside surface.  This indicates the blank in a drop should be placed with the texture up, facing the heating elements.  The smoother side facing the floor will be stretched and will remain smooth. 

The smoothing effect of firing with rough side up does depend a little on the depth of the drop.  Shallow drops will not have the same heat exposure that deeper drops do, assuming that a moderate heat is being used over three to four hours.

This implies that the design to show on the inside of the drop should be in contact with the separator when fusing the blank.

Firing Records

Bullseye Glass Company

To develop your fused glass practice, you need to record lots of information about your firings.  This tells you what has gone well and not so well.  It hones your expectations about how you should be preparing, scheduling, and analysing your experiences.  It becomes your detailed memory bank of results and gives directions for the future.  This should be done whether fired in your own kiln or someone else’s.

Categories of information for the record
There is quite a bit of information that needs to be included in such a record.  This is my view of what needs to be included  in your logbook for future reference.

Date
Record the date of the firing as that will give you historical information on similar projects.  It can show you what you have changed over time and the variations you have introduced.

Glass used
This is not only the type of glass (Bullseye, Float, Oceanside, Wissmach, Youghiogheny, etc), but the colours used.  This should include the manufacturer’s code numbers to enable you to replicate the glass used.

Lay up
This can be a description, a drawing or pictures of the set-up of the piece prior to firing.  This is vital to later understanding what you did in this firing.  Record any glues or stabilising elements you use. Any frits or powders used should be recorded. The placement in the kiln is important - centred, one corner or another, level/ height in kiln, etc., can affect the results.  You can make a sketch or take a photo to attach to the record rather than writing separate descriptons. How it comes out is recorded later.

Dimensions
The dimensions (h x w x d) including any variations in height are needed to compare with other projects.  This might be included in the lay-up diagrams or pictures, but it is most useful to have the dimensions and their variations recorded as numbers too.  You might think in terms of layers, but remember to record the thickness of each layer/piece (e.g., 2mm, 3mm, 4mm, 6mm, etc)

Kiln used
This is especially important if the kiln is not yours. Every kiln has variations and it is important to compensate for that in scheduling and placing of the piece in the kiln.

Process
This is essential in gaining an understanding for planning any modifications.  The process can be described by standard terms - e.g.,  sinter, slump, tack, contour, full fuse, casting, melt – or by your own terminology (if it is consistent).

Description
A statement of your project and aims is very useful for the future.  It is a reference point to use in comparing what you wanted with the results of the firing.

Support system
This includes essential information affecting the firing – shelf type (e.g., fibre, mullite, ceramic tile), mould type (e.g., ceramic, fibre, steel), and a description or sketch including any reference codes.

Kiln furniture. The kind and quantity of kiln furniture (dams, stilts, posts, etc) can affect the firing results, so need to be recorded.

Separators
This includes kiln wash (type, whether new or the number of uses), fibre paper type and amount, mould coatings, and anything else you may use to keep the glass from sticking.

Schedule
This is the thing most everyone remembers to record.  You need to record it each time you use it – even if you have used it many times before.  You need to record each step of the program.

So many times, people report that “it [the schedule] has always worked before”, only to discover that some element had been intentionally or accidentally altered from past firings.  I normally write the schedule in a logbook and then enter it into the programmer. I use the written record to check against what I have entered into the controller.  Then I know I have programmed what I intended.  I can also check on earlier, similar firings to see the variations I have used in the past.

Results
Drawings or pictures of the finished item are essential.  A description of the results is also needed as a picture does not tell the whole story.

Comments on results
You should also give a commentary on the results of the firing.  This should include successes as well as disappointments.  Thoughts for future similar firings should be written down.  They will be forgotten soon, if you don’t.

How to keep all this information
As you can see there are many elements that need to be recorded as they each can affect a firing. I see these as a minimum, and you will add elements important to you for this list.

It does not matter much in what form you keep the information.  It can be a ledger, spreadsheet, database or your phone or tablet that you carry with you always.  There are several apps for recording the kiln firings that can be used.  What is important is that you can record the information immediately, or as you prepare the work for the kiln, into the chosen form of recording.  I use a logbook and convert that in my leisure moments to a spreadsheet (usually at new years day).  This allows me to compare information over time and especially the kinds of firings that I rarely do.  It also allows me to search by various processes.

It is important that you back up any electronically held information to the cloud or other device to protect against loss or corruption. 

Forms
It is useful to have a form for compiling this record.  A number of elements of the records can be reduced to tick boxes to ease the recording.  It helps to remind you of the information you need to log for each firing.  Bullseye have an excellent form that you can use or adapt to your needs. There are a few apps that can be used on phones or tablets which are useful for those who record everything on their phone.  Remember to back it all up to the cloud for preservation in case of loss or damage.

As Fast as Possible Firings

I have long advocated that it is best to avoid as fast as possible firings because the way controllers work.  They compare the temperatures several times a minute (the number depending on the manufacturer) to determine the rate of increase.  This allows big overshoots at the top temperature with fast rises.  This was reinforced this morning by observing a different factor.
 
I took a piece out at 68°C to put another in.  During the time the kiln was open, the air temperature dropped to 21°C.  I filled the kiln and closed the lid and idly watched the temperature climb before switching the kiln on for another firing.  It took a bit more than two minutes for the thermocouple to reach 54°C with the eventual stable temperature being 58°C.  I had not been aware how long it takes the thermocouple to react to the change in temperature.  Yes, it takes a little time for the air temperature in the kiln to equalise with the mass of the kiln, but not two minutes.
 
With a two-minute delay the recorded temperature can be significantly behind the actual air temperature.  For example, a rate of 500°C per hour is equal to 8.3°C (15°F) per minute or 16.6°C (30°F) overshoot of the programmed temperature. Even at 300°C it is a 10°C (18°F) overshoot.  This effect, added to the way the controller samples the temperatures, means the actual overshoot can be significant for the resulting glass appearance.
 

This is just another small element in why moderate ramp rates can be helpful in providing consistent results for the glass.

Darkening leads

There are several ways to darken the leads in leaded panels. Three are to:

use patina on the leads,

brush with on stove blackening with a soft brush, and

simply brush after cementing.

A certain number of people use black patina to darken the leads after cementing and cleaning the panel.  This certainly gives a black result, but it introduces an acid to the panel. I do not do this, nor do I recommend it.

Another method of darkening is to apply stove blackening or black oil paint to the panel to make the leads dark.  I recommend that you put very small amounts on a soft brush and then brush over the leads.  It might have to have a little more colour added for a large panel, but that is better than having to clean up large areas of smudged black over the glass, especially with painted glass.

credit: PicClick UK

But...

You can darken lead came without patina or black colour.  You finish the panel with the scrubbing brush to push whiting against the fillet of lead light cement against the leads as normal.  This has the effect of cleaning the glass as well as stiffening the cement at the edge of the cames. Remove the excess whiting as normal.

But, before picking out all the excess cement once the scrubbing brush process is finished, use a soft brush, such as a shoe brush, over the whole panel.  This can be mechanised by using a soft bristled mop in a drill motor on a slow to medium speed.  This will pick up colour from the cement and spread it evenly over the lead and solder joints. It will give a dark grey appearance to the whole of the leading and solder joints as well as polish up the glass. 

The degree of shine will be dependent on the amount of time you wish to spend, but can be a polished to a very dark grey to black colour.  This will last longer than simple black colour brushed onto the leads, as it is bound by the linseed oil in the cement to the surface of the leads. Also, it quickly dries so that not so much black is transferred to your hands as you handle it.

Making lead cames black during the finishing of a leaded panel is as simple as brushing over the cames before picking out all the excess lead light cement.