Sample Tiles

credit: Tia Murphy

There are advocates for making tiles as references for future work.  

• They show the profiles achieved at different temperatures.  
• They can be stored for easy visual reference when planning a firing.  
• It is a useful practice for any kiln new to the user.  

These tiles are assembled in identical ways to enable comparisons.  They should include black and white, iridised pieces- up and down, transparent and opal, and optionally stringers, confetti, millefiori, frit and enamels.  

The tiles are fired at different top temperatures with the same heat up schedule with the top temperature of each at about 10C or 20F intervals.  These show what effect different temperatures give.  Start the temperature intervals at about 720C or 1330F.

This is a good practice, even if time consuming.  It gets you familiar with your kiln and its operation.  It gives a reference for the profiles that are achieved with different temperatures at the rates used.

Ramp rate and time

But, as with many things in kilnforming, it is a little more complicated.  The effect you achieve is affected by rate and time used as well as the temperature.

The firing rate is almost as important as the temperature.  

• A slow rate to the same top temperature will give a different result than a fast rate.  
• The amount of heat work put into the glass will affect the temperature required.  
• Slow rates increase the time available for the glass to absorb the heat.  
• Glass absorbs heat slowly, so the longer the time used by slower rates, the rounder the profile will be.

Since time is a significant factor in achieving a given profile, any soaks/holds in the schedule will affect the profile at a set temperature.  A schedule without a bubble squeeze will give a different result than one with a bubble squeeze at the same temperature.

To help achieve knowledge of the rate/time effect, make some further test tiles.  Use different rates and soaks for the test tiles of the same nature as the first temperature tests. But vary only one of those factors at a time. Consider the results of these tests when writing the schedule for more complex or thicker layups. 

Mass

Also be aware that more mass takes longer to achieve the same profile.  Slower rates and longer times will help to achieve the desired profile at a lower temperature.  It is probably not practical to make a whole series of test tiles for thicker items.  But, a sample or two of different thicknesses and mass will be helpful to give a guide to the amount of adjustment required to achieve the desired outcome.

The results of sample tiles are due to more than just temperature.  They are a combination of rate, time, and temperature (and sometimes mass).  These factors need to be considered when devising or evaluating a schedule, because without considering those factors, it is not possible to accurately evaluate the relevance of a suggested top temperature.

See also: Low Temperature Kilnforming, available from Bullseye and Etsy

Scheduling for Thick Landscapes

Thick slabs often involve numerous firings of increasingly thick work.  I am using an existing example, with their permission, of the first stages of a thick landscape.  The initial concern was with bubbles in the first layup, then the strategy for firing the thick slab.

Plans

This is the first part of a landscape with depth.  It will be fired 5-7 more times.  This first piece will be inverted for the next firing with the clear facing up, to avoid reactions between the colours.  It is similar to an open face casting. There is a Bullseye Tip Sheet on open face casting that will give a lot of information.

Layup

Picture credit: Osnat Menshes

This work has a base of clear that is mostly overlaid with one layer of 3mm pieces, although in some places another layer, and there are some pre-fired elements as well.  It is fired on Thinfire shelf paper.

Bubbles 

There is concern about the number and size of the bubbles after the firing, and how to avoid them.  Will they grow over the multiple firings?

The many small bubbles are characteristic of kilnformed glass.  The few larger bubbles may result from the frit that is under the pieces that form the top surface.  And there are some overlaps of clear over colour that may form pockets where air can collect. I advise leaving the scattering of the frit until all the decorative pieces are in place.  The bubbles will migrate toward the top during the multiple firings.  They will not grow in size unless they combine during the upward migration.  A later suggestion about reducing the number of firings will reduce the bubble migration and risk of increasing in size.

Picture credit: Osnat Menshes

Schedule

Proposed Schedule (Temperatures in degrees Celsius)

1: 180 – 560, 30’    I would go to 610 for 30'

2: 25 – 680, 120’    I would use only 30'

3: 220 – 810, 15’    I would set the top temperature at 816, 15’.

4: 9999 – 593, 30’  Eliminate this segment. 

5: 9999 – 482, 120’ I suggest one hour soak

8: 55 – 370, off      83 – 427, 0’

7: 150 – 371, 0’

8: 330 – to room temperature, off.

 

Eliminate segment number 4.  Any temperature equalisation done at this temperature, is undone by the AFAP to the  annealing.  The temperature equalisation occurs at the annealing temperature. No soak at an intermediate temperature is required.  This blog post gives some information about annealing above and below the annealing point (Tg). 

Firing Incremental Layers

The plan is for five to seven more firings.  Continuing to build up the thickness on each firing, may have some problems.

• There is increased risk of compatibility problems when firing a piece to full fuse many times.
• There is a risk of more bubbles and of the existing ones becoming larger as they move upwards and combine with other smaller ones.
• With each firing the thickness is increasing and so becoming a longer firing.  This is because the heat up, annealing, and cooling each need to be longer.  For example - 6mm needs 3hour cooling, 12mm needs 5 hours, 19mm needs 9 hours. 

Multiple Slabs

These are the main reasons that I recommend firing a series of 6mm slabs separately and combining them in one final firing.  Firing a series of 6mm slabs and then combining them in a single long and slow final firing has advantages.

• The individual pieces do not need to go through so many full fuse firings, reducing the risk of compatibility problems.
• The small bubbles in each firing will not have the chance to rise through all the layers to become larger.
• The total time in the kiln for the combined pieces will be less than adding layers to already fired layers.

Examples

It is often difficult to convince people that firing by adding incrementally to an existing slab, longer firing times are required than by firing a group of 6mm slabs and a single combined firing of all the slabs.  I give an example to illustrate the differences.

Annealing

Assume there are to be a total of eight firings (existing 6mm slab and 3mm for each of seven more firings).  Also assume that each additional firing is of 3mm. This makes a total of 28mm.  Compare annealing and cooling times for each firing:

Firing      thickness       anneal and cool (hours minimum)

1            6mm                    3

2            9mm                    4

3            12mm                   5

4            15mm                   7

5            18mm                   9

6            21mm                   11.5

7            25mm                   14

8            28mm                   17

Total                                   70.5 hours annealing time (minimum)

To fire up 5 six millimetre slabs takes less time – 3 hours annealing and cooling time for each firing cumulates to 15 hours.  Add to that the final firing of 17 hours annealing time.  A total of 32 hours.  This is half the time of adding to the existing slab at each firing.  Multiple 6mm slabs can be fired at the one time if there is space in the kiln, which would reduce the kiln time for the 6mm slabs even further. 

An additional advantage of firing 6mm slabs and combining them, is that bubbles can be squeezed out more easily in the final thick slab fring because of the combined weight of the  slabs.  You could make the individual slabs a little thicker, but that would involve damming each slab.  Not an impossible task of course.  And it would change the calculations, by reducing the number of firings.

Heat Up

Another time saving is to use the second cooling rate from the Bullseye document Annealing Thick Slabs as the first up ramp rate. Take this rate up to a minimum of 540˚C. Although, this is an arbitrary temperature above the strain point to ensure all the glass is above the brittle phase.  It is possible to maintain this initial rate to the bubble squeeze.  But with the slow rises in temperature required for thicker slabs, it is sensible to increase the rate from 540 to bubble squeeze to reduce the firing time.  Once past the bubble squeeze a more rapid rate can be used to the top temperature.  

The heat up times could be about half the minimum cooling times.

A worked example (with certain assumptions) would be:

Firing      thickness       time to top temperature total time.

1            6mm             6.3               

2            9mm             7.1

3            12mm            8.4

4            15mm            10.7

5            18mm            15.9

6            21mm            19.4

7            25mm            25.1

8            28mm            29.1              ca.122 hours

But firing five times for 6mm equals 31.5 hours plus the final firing up of 29.1 hours equals a total of 60.6 hours.  Again about one half the time of progressively building up a base slab to the final thickness.

Savings

This example shows that approximately 90 hours of firing time can be saved by making a series of six millimetre slabs and combining them in a final firing.  There is the additional advantage of reducing the occurrence of bubbles between the layers in the final firing because of the weight of the combined slabs.

Heat Up Soaks

Photo credit: Bullseye Glass Co.

It is often advocated that there should be a soak at the strain point to even out the temperature throughout the glass.

My question continues to be why? 

The glass has survived whatever rate has been used up to that point during its brittle phase.  So, it already has every chance of surviving a rapid rate during the plastic phase.

Instead of a soak at the strain point, Bob Leatherbarrow indicates a soak during the brittle phase will be more successful in avoiding heat up breaks.  He has observed that heat up breaks are most likely to happen around 260ºC/500ºF.  Therefore, a soak in that region is most likely to be of use in evenly distributing the heat effectively through the glass rather than at a higher temperature.  He recommends up to a half hour soak there before proceeding at the same rate to the strain point (about 540ºC/1004ºF).  The ramp rate to this heat up soak in the brittle phase should be related to the thickness of the glass and the intended profile.

The thickness to be fired for is determined by the profile.  Rates for full and contour fusing can be as for the thickness before firing.  Rounded tack fuse needs to be fired as though twice as thick, and sharp tack or laminated fuse need to be fired as though 2.5 times.  More information on initial ramp rates to the strain point can be found in Low Temperature Kilnforming available from Bullseye and from Etsy

Deep Slumps with Bubbles

 

Photo Credit: Rachel Meadows-Ibrahim

The main causes of the large thin bubble is most probably  too high a temperature combined with a long soak.

Elevation of the Mould

The poster indicated there are eight holes total – four on the sides and four under the glass. This means any air has an exit out from under the glass and from the inside of the mould. So, in this case it does not need to be elevated for exit of air.  In my practice l have never, except in tests, elevated my slumping moulds. I have not had failures. My experiments involved in writing the eBook Low Temperature Kilnforming  showed no significant temperature differences between elevating, or not, below the mould.

Effect of Fast Rates

Slow rates to low temperatures with long soaks avoid sealing the glass to the mould. This means air can move out from under the glass during the slump. 

• Fast rates, and elevated temperatures can restrict air movement from under the slumping glass.  
• Fast rates and high slump temperatures can each cause uprisings because the glass slides down the mould during the soak, and that weight pushes the bottom upwards.

Temperature and Uprisings

This uprising is different from the bubble at the bottom on this piece. It is possible to see the glass bubble is thinner than the surrounding glass. As there were holes for air to escape, it seems the temperature and or speed was great enough to allow the glass to form to the mould at the bottom.  This covered the air holes and allowed the remaining air to push upwards on the glass.  A lower top temperature may have avoided this bubble formation.  Certainly, a combination of a slower rate and a lower temperature would have avoided the formation of the bubble.

Observation

Further, observation during the firing would have caught this bubble formation early enough to skip to the annealing and result in a piece with only a slight uprising, and before it became a bubble. Peeking should start at the beginning of the slumping soak and be repeated at 5 to 10 minute intervals.

Visible Devitrification

"Why does devitrification appear on slumped pieces?"

A brief explanation 

Scientific research in developing a glass matrix to support bone grafts gives some information.  This kind of glass matrix requires to be strong.  Development showed that devitrification weakens the matrix.  The crystals in a matrix are not as strong as the amorphous glassy state.  So, devitrification needs to be avoided.

The research to avoid devitrification showed that it begins at about 600˚C/1110˚F.  It only begins to become visible above 700˚C/1300˚F.  The process developed was to introduce a “foaming” agent.  The process fired slowly to 600˚C/1110 ˚F and then quickly to 830˚C/ 1530˚F.  It left a strong open matrix around which bone can grow. Although the research used float glass, it is also a soda lime glass, just as fusing glasses are.  The formation of devitrification begins at the same temperature for fusing glasses as for float.

The result of this medical research shows that devitrification begins on glass before it is visible. Devitrification is cumulative. A little becomes greater with another firing.  This is so even with good cleaning between firings. The new devitrification builds on the previous.  It does this from 600˚C/1110 ˚F.

A subsequent firing can continue this devitrification to the point where it is visible. This can happen, although the temperature at which we can see it after one firing has not been reached.  This continued devitrification at low temperatures can become great enough to be visible at the end of one or multiple slumps.

Credit: Bullseye Glass Co.

What can we do?

Clean all the glass before every firing very well.

·         Avoid mineralised water.

·         Final clean with isopropyl alcohol.

·         Polish dry at each stage with white absorbent paper.

 

Soak longer at lower temperatures.

·         Use longer soaks to achieve the slump.

·         Keep the temperature low.

·         Observe the progress of the firing with quick peeks.

 

Use slower ramp rates.

·         Slower rates enable the heat to permeate the glass.

·         Enables a lower slump temperature.

 

If there is any hint of devitrification after the first firing,

·      use a devitrification spray, or

·      provide a new surface.

• o   remove the surface by abrasion on sandblasting,
• o   cap with clear, or
• o   cover whole surface with a thin layer of clear powder.

·      Fire to contour fuse to give a new smooth surface.

·      Clean very well and proceed to slump.

Slower Ramps on Additional Firings

"Every time you fire a previously fired piece you need to slow down."

This is not accurate. If you have not changed anything significant, the annealing does not need to be extended.  The clearest example is a fire polish.  Nothing has been added. The physics and chemistry of the piece have not changed.  If only confetti or a thin frit/powder layer is added, nothing significant for scheduling has been added.  As nothing significant has changes the annealing used in the previous firing can be used again.

Of course, you do need to slow the ramp up rates on the second firing.  This is because you are firing a single thicker piece.  On the first firing, the pieces are individual and can withstand slightly faster rates. But on third and subsequent firings, if nothing significant has been changed, there is no need to slow rates further.

There is a post which describes this further.

"When adding more thickness more time is needed."

This is the occasion when the annealing soak needs to be extended.  Placing a full sheet of clear glass on the bottom, or less usually, the top, and taken to a full fuse, requires slower ramp rates.   The annealing time for a full fuse can be taken directly from the annealing tables for thick slabs.  

The fusing profile for any additional items has a strong affect on the length of the annealing soak.  If the glass is now of uneven thicknesses, and greater care in assigning ramp rates is needed.  The profile for the piece also determines the amount of additional annealing time required.  A sharp tack of a single additional layer will require annealing as for 2.5 times the total height of the piece at the start or the firing. A rounded tack will need two times and a contour fuse will require 1.5 times.  A full fuse can be carried out for the new total height of the piece without any multiplying factors.

 If the intention with multiple firings is to achieve a variety of profiles within one piece, a slightly different approach is required.  A blog post here describes the process.

The general approach to multiple firings is that unless there are changes to the thickness or profile of the glass, no changes in annealing time is required.  

 

Slow Rates to Annealing

"I have seen recommendations for slower than ASAP rates from the top temperature, but most schedules say 9999 or ASAP.  Which is right?"

Slow drops in temperature from top to annealing temperatures risk devitrification. Accepted advice is to go ASAP to annealing temperature to avoid devitrification forming.

Breaks do not occur because of a too rapid drop from top temperature to annealing. The glass is too plastic until the strain point has been passed to be brittle enough to break. On the way down that will be below an air temperature of 500˚C/933˚F.

credit: ww.protolabs.com

Different kilns cool from top temperature at different rates. Ceramic kilns are designed to cool more slowly and may need assistance to cool quickly.  This is usually by opening vents or even the door or lid a little. Glass kilns are designed to lose temperature relatively quickly from high temperatures. They do not need a crash cooling as ceramic kilns may need in certain circumstances.  Of course, crash cooling may be necessary for some free drops and drapes.

The length of the soak at annealing is determined by the effective thickness of the piece.  Tack fusing needs to be annealed for thickness as a factor of 1.5 to 2.5, depending on profile.

The extent to which you control the cooling to room temperature after the anneal soak is dependent on the calculated thickness of the piece you are cooling. The objective is to keep the internal temperature differential to 5˚C/10˚F or less to avoid expansion/ contraction differences that are great enough to break the piece. Those rates are directly related to the required length of the anneal soak.  Those rates can be taken from the Bullseye chart for Annealing Thick Slabs. The Fahrenheit version is is available too.

An example.  If you have a 2 layer base with 3 layers (=15mm) stacked on top for a rounded tack fuse, you need to fire as for at least 30mm. This will require controlled cooling all the way to room temperature.

• ·        The rate to 427˚C /800˚F will be19˚C /34˚F
• ·        The rate to 370˚C /700˚F will be 36˚C /65˚F
• ·        The final rate 120˚C /216˚F to room temperature.

You may need to wait a day before any coldworking. An example from my experience shows the necessity.  I checked a piece for stress a few hours after removing the piece from the kiln when it felt cool to the touch. It puzzled me that stress showed, although it didn't on similar pieces.  The next morning, I went to check if I misunderstood the reading. Now, a full 15 hours after coming out of the kiln, there was no stress.  The example shows that the glass internally is hotter than we think. And certainly, hotter than the air temperature.

In the temperature regions above the strain point, the glass needs to be cooled quickly. In the annealing region and below the glass needs to be cooled slowly.

More information is available in the eBook Low temperature Kilnforming.  This is available from Bullseye or Etsy

Heat Up vs Annealing

I am amazed by the effort put into ramp up rates, bubble squeezes, and top temperatures in comparison to annealing.  The emphasis on social media groups seems to be to get the right ramp rates for tack fuses and slumps, bubble squeezes, etc.  Most of the attention is on the way up to processing temperature.

The treatment of annealing and cooling is almost cavalier by comparison.  The attention seems to be on what temperature, and how long a soak is needed.  Then some arbitrary rate is used to cool to 370ºC/700ºF.

Annealing, in comparison to firing to top temperature, is both more complex and more vital to getting sound, lasting projects completed.  Skimping on annealing is an unsound practice leading to a lot of post-firing difficulties.

Annealing is more than a temperature and a time.  It is also the cooling to avoid inducing temporary stress. That stress during cooling can be large enough to break the glass.  This temporary stress is due to expansion differentials within the glass.

People often cite the saving of electricity as the reason for turning off at 370ºC/700ºF.  My response is that if the kiln is cooling off slower than the rate set, there will be no electricity used.  No electricity demands.  No controller intervention.  No relay operation.

Annealing at the lower end of the range with a three-stage cooling provides good results.  The results of Bullseye research on annealing are shown in their chart for annealing thick items.  It applies to glass 6mm and much larger.  It results from a recommendation to anneal at the lower end of the annealing range to get good anneals.  Other industrial research shows annealing in the lower end gives denser glass, and by implication, more robust glass.  Wissmach have accepted the results of Bullseye research and now recommend 482ºC/900ºF as the annealing temperature for their W96.  The annealing point of course remains at 516ºC/960ºF.

Bullseye research goes on to show that a progressive cooling gives the best results.  They recommend a three-stage cooling process.  The first is for the initial 55ºC/º100F below the annealing temperature, a second 55ºC/100ºF cooling and a final cooling to room temperature.

It is a good practice to schedule all three cooling rates.  It may be considered unnecessary because your kiln cools slower than the chart indicates.  Well, that is fine until you get into tack and contour fusing.  Then you will need the three-stage cooling process as you will be annealing for thicknesses up to 2.5 times actual height.

 

Of course, you can find out all the reasons for careful annealing in my book "Annealing; concepts, principles, practice" Available from Bullseye at

https://classes.bullseyeglass.com/ebooks/ebook-annealing-concepts-principles-practice.html

Or on Etsy in the VerrierStudio shop

https://www.etsy.com/uk/listing/1290856355/annealing-concepts-principles-practice?click_key=d86e32604406a8450fd73c6aabb4af58385cd9bc%3A1290856355&click_sum=9a81876e&ref=shop_home_active_4

Refiring and Annealing

A question about re-fusing: 

I have just taken a large piece, with uneven layers out of the kiln, it went in … and fired for double thickness. A small piece has flipped and is showing the white side. … If I cover this with a thin layer of coloured powder frit, does the piece need the long anneal process when I fire it again, please. I will be taking it up to the lowest tack fuse temperature possible [my emphasis], so the rest doesn’t change too much.

When considering the re-firing of a fused piece, even with minimal changes, the schedule needs re-evaluation of both ramp rates and annealing. In this case, the major change is using a sinter firing – “the lowest tack fuse temperature possible”.

Ramp Up Rates

Previously the piece was in several layers.

• The piece is now a thicker single piece and needs more careful ramp rates.
• It is also of uneven thicknesses.
• And you intend to fire to a sharp tack or sinter.

These things make a requirement for more cautious firing. You cannot fire as quickly from cold as forthe original unfired piece. Previously, the sheets could be heated as though separate. They were not hot enough to stick together until beyond the strain point. They now could experience the differential expansion from  rapid heating, which can cause breaks. 

The previously fired piece will need a slower initial ramp rate this time. This is because you are firing for a sharp tack. This is also known as fusing to stick, or sintering. It is not because of a second firing. It is because of the differences in the glass for this firing. You are firing a single thicker piece of uneven layers to a sharp tack.

Looking at Stone* and the Bullseye chart for Annealing Thick Slabs indicates that in general, the first ramp rate should be halved for each doubling of calculated thickness. This is for full fused items. However, this is going to be a more difficult fusing profile - sintering. The calculation for sintering is as for 2.5 times the thickest part of the piece. This factor of 2.5 was determined by a series of experiments that are detailed in the eBook Low Temperature Kilnforming.

You started with firing two layers of 3mm/0.125” at possibly 330°C/595°F. You are now firing the fused 6mm/0.252 piece to a sharp tack. This means you should be looking at firing for 2.5 times or 15mm/0.625”. This implies 240°C/435°F as the maximum first ramp rate. A more cautious approach is to fire to 300ºC/540ºF at a rate of 72ºC/130ºF, as most heat-up breaks occur below that temperature. You should maintain that rate to 540°C/1005°F afterwards. 

Annealing

The annealing time and cool rate will be affected in the same way as the change to a sharp tack firing. Without that fuse profile change, and no change in the profile or thickness of the piece, it could have been annealed as previously. However, changing to a sharp tack means a longer anneal soak is required. This sharp tack annealing is for 2.5 times the thickness or 150 minutes.

Cooling

The cooling rates for this piece are not the same as for the first firing. A sharp tack firing will require cooling rates of:

• 40ºC/73ºF to 482°C/900°F.
• 72ºC/130ºF f427ºC/800ºF.
• 240ºC/435ºF to room temperature

This applies regardless of the fusing glass you are using, as it is the viscosity which is the important factor in cooling.  Viscosity is primarily related to temperature.

Refiring with Significant Additions.

Ramp rate

If there are additions to the thickness, a slower first ramp rate will necessary. If an additional 3mm layer is placed on top of a 6mm base for a rounded tack, you will need to schedule as for 19mm/0.75” (twice the thickest part). This will be 150°C/270°F for the first ramp rate. For a sharp tack, it will be as for 22.5mm/0.825”. The maximum rate will be reduced to 120ºC/216F for the first ramp. This shows the additional caution required for sharper fusing profiles.

Annealing

The annealing will need to be longer than the first firing. The thickness has changed with the additions of pieces for a rounded tack firing. Instead of annealing for 6mm/0.25” you will be annealing as for 19mm/0.75”. This requires a hold of three hours at the annealing temperature and cooling over three stages:

• The first cool rate is 25°C/45°F per hour to 482°C/900°F.
• The second rate is 45°C/81°F per hour to 427ºC/800ºF.
• The last rate is at 90C°C/162°F per hour to room temperature.

If there are additions, plus firing to the lowest possible tack temperature – as in the example - the firing must be as for 2.5 times the actual thickness. Annealing as for 25mm/1” gives rates of:

• The first cool rate is 15°C/27°F per hour to 482°C/900°F.
• The second rate is 27°C/49°F per hour to 427ºC/800ºF.
• The last rate is at 90C°C/162°F per hour to room temperature.

These examples show how dramatically later additions in thickness can add to the length of the firing to re-fire a well-annealed piece without breaking it on the heat-up. It also shows that changing the profile to a sharper tack affects the annealing and cooling times and rates.

 

*Graham Stone. Firing Schedules for Glass; the Kiln Companion. 2000, Melbourne. ISBN 0-646-397733-8

As a side note Stone’s book has become a collectable.

Scheduling with the Bullseye Annealing Chart

This post is about adapting the Bullseye chart Annealing Thick Slabs to write a schedule for any soda lime glass as used in kilnforming.

I frequently recommend that people should use the Bullseye chart for Annealing Thick Slabs in Celsius  and Fahrenheit.  This chart applies to glass from 6mm to 200mm (0.25” to 8”).

“Why should the Bullseye annealing chart be used instead of some other source?  I don’t use Bullseye.”

My answer is that the information in the chart is the most thoroughly researched set of tables for fusing compatible glass that is currently available.  This means that the soak times and rates for the thicknesses can be relied upon.

“How can it be used for glass other than Bullseye?”  

The rates and times given in the chart work for any soda lime glass, even float. It is only some of the temperatures that need to be changed.

"How do I do that?"  

My usual response is: substitute the annealing temperature for your glass into the one given in the Bullseye table.

 "It’s only half a schedule."

That is so.  The heating of glass is so dependent on layup, size, style, process, and purpose of the piece.  This makes it exceedingly difficult to suggest a generally applicable firing schedule.  People find this out after using already set schedules for a while. What works for one layup does not for another.

Devising a Schedule for the Heat Up

There is no recommendation from the chart on heat up.  You have to write your own schedule for the first ramps.  I can give some general advice on some of the things you need to be aware of while composing your schedule.

The essential element to note is that the Bullseye chart is based on evenly thick pieces of glass.  Tack fusing different thicknesses of glass across the piece, requires more caution. The practical process is to fire as for thicker pieces.  The amount of additional thickness is determined by the profile being used.  The calculation for addition depends on the final profile.  The calculation for thickness is as follows:

• Contour fusing - multiply the thickest part by 1.5. 
• Tack fusing - multiply the thickest part by 2. 
• Sharp tack or sinter - multiply the thickest part by 2.5.

The end cooling rate for the appropriate thickness is a guide for the first ramp rate of your schedule.  For example, the final rate for an evenly thick piece 19mm/0.75” is 150ºC/270ºF.  This could be used as the rate for the first ramp. 

Bob Leatherbarrow has noted that most breaks occur below 260ºC/500ºF.  If there are multiple concerns, more caution can be used for the starting ramp rate.  My testing shows that using a rate of two thirds the final rate of cooling with a 20 minute soak is cautious.  In this example of a 19mm piece it would be 100ºC/180ºF per hour.

Even though for thinner pieces the rates given are much faster, be careful.  It is not advisable to raise the temperature faster than 330ºC/600ºF per hour to care for both the glass and the kiln shelf.

Once the soak at 260ºC//500ºF is finished, the ramp to the bubble squeeze should maintain the previous rate.  It should not be speeded up.  The glass is still in the brittle phase.

After the bubble squeeze you can use a ramp rate to the top temperature of up to 330C/600F.   AFAP rates to top temperature are not advisable.  It is difficult to maintain control of the overshoots in temperature that are created by rapid rates.  

The top temperature should be such as to achieve the result in 10 minutes to avoid problems that can occur with extended soaks at top temperature.

In the example of an evenly thick 19mm/0.75” piece a heat up full fuse schedule like this could be used:

• 150ºC/270ºF to 566ºC/1052ºF for 0 minutes
• 50C/90F to 643C/1191F for 30 minutes
• 333ºC/600ºF to 804ºC/1479ºF for 10 minutes

 

If a more cautious approach to the heat up is desired, this might be the kind of schedule used:

 

• 100ºC/180ºF to 260ºC/500ºF for 20 minutes
• 100ºC/180ºF to 566ºC/1052ºF for 0 minutes
• 50C/90F to 643ºC/1191ºF for 30 minutes
• 333ºC/600ºF to 804ºC/1479ºF for 10 minutes

This approach is applicable to all fusing glasses.

 

Adapting the Bullseye Annealing Chart

After writing the first part of the schedule, you can continue to apply the annealing information from the Bullseye chart.  The first part of the anneal cooling starts with dropping the temperature as fast as possible to the annealing temperature.

The method for making the chart applicable to the annealing is a matter of substitution of the temperature.  All the other temperatures and rates apply to all fusing glasses.

Use the annealing temperature from your source as the target annealing  temperature in place of the Bullseye one.  The annealing soak times are important to equalise the temperature within the glass to an acceptable level (ΔT=5ºC).  The annealing soak time is related to the calculated thickness of the piece.  This measurement is done in the same way as devising the appropriate rate for heat up. 

Applying the Cooing Rates

Then apply the rates and temperatures as given in the chart.  The three stage cooling is important.  The gradually increasing rates keep the temperature differentials within acceptable bounds with the most rapid and safe rates.

The temperatures and rates remain the same for all soda lime glasses – the range of glass currently used in fusing, including float glass.  The soak time for the calculated thickness of your glass piece will be the same as in the Bullseye chart.  

This means that the first cooling stage will be to 427ºC/800ºF.  The second stage will be from 427ºC/800ºF to 371ºC/700˚F.  And the final stage will be from 371ºC/700˚F to room temperature.

I will repeat, because it is so important, that the thickness to be used for the anneal soak and cooling rates for your schedule relates to the profile you desire.  A fuse with even thickness across the whole piece can use the times, temperatures, and rates as given in the chart as adapted for your glass.  The thicknesses to use are for:

Contour fusing - multiply the thickest part by 1.5. 

Tack fusing - multiply the thickest part by 2. 

Sharp tack or sinter - multiply the thickest part by 2.5.

An annealing cool schedule for 19mm/0.75" Oceanside glass is like this:

• AFAP to 510˚C/ 951˚F for 3:00 hours
• 25˚C/45˚F to 427˚C/800˚F for 0 time
• 45˚C/81˚F to 371˚C/700˚F for 0 time
• 150˚C/270˚F to room temperature, off.

Many will wish to turn off the kiln as early as possible.  This is not part of best kilnforming practice.  If you still wish to do this, the turn off temperature must be related to the thickness and nature of the piece.  To turn off safely, you need to know the cooling characteristics of your kiln.  This can be determined by observing the temperature against time and then calculating the kiln’s natural cooling rate. And then applying that information to cooling the kiln.

 

The best source for devising schedules is the Bullseye chart for Annealing Thick Slabs.  It is well researched and is applicable with little work to develop appropriate schedules for all the fusing glasses currently in use.