Bubble Mystery

A question was asked about a collapsed bubble. There were two pieces in the kiln and one (strips) was fine and the other (flat plate) had the collapsed bubble.  Both on the same dried shelf.  The question also asked if the collapsed bubble piece could be flattened by fusing again.

Collapsed Bubble

The bubble collapsed because it had not burst by the time the cool toward annealing had begun.  As the air pressure under the bubble dropped, and the weight of the thinned glass bubble sank down as there was not enough air pressure to hold it up.

The glass is now thinner at the centre of the bubble than the main part of the piece, and thicker at the edge of the bubble. I don't think it is possible to successfully flatten it to become an even thickness across the whole piece. To get the same thickness across the whole piece would require high temperatures and long soaks there. 

Another possibility is to use a pressing solution. 

My suggestion is to add elements or repurpose it. I don’t think any repairs would present a good-looking piece.

Diagnosis

The on-line diagnosis of the possibilities for the cause of the bubble was extensive and sometimes inventive.  It was finally determined the bubble was from under the glass, that is, between the glass and the shelf. A slight depression in the shelf is the usual explanation.  The user tested the shelf for smoothness and found no depressions.

It was clear the bubble came from under the glass.  All the suggestions about how bubbles can form under glass were given, but none seemed to apply.

How can you get a bubble on a dry shelf that is perfectly flat and that has not been subjected to too rapid or too high a temperature?

Solution

The answer is that a little spot of grit or tiny ball of fibre paper can keep the glass raised up enough for air to be trapped.

Prevention

It is not enough to test the shelf is flat.  You need to use clean kiln wash with a clean brush to avoid any grit being brought to the shelf. It is also a good reason to vacuum the shelf before each use in case any dust or grit has fallen onto the shelf. Covering the shelf or putting it into a cupboard will also reduce the possibility of small bits of grit falling onto the shelf.

Of course, if you smooth the kiln wash with a nylon or similar fine cloth, you will remove any specks of grit.  A vacuum of the shelf after smoothing is still a good idea.

Conclusion

It is as important to keep tools and materials clean as it is to clean the glass you are going to kilnform.

Sand Beds for Kilns

Sand beds can be used for shaping directly into the sand or as a bed for a large kiln to avoid having to place a number of shelves together and patch cracks. It also saves on the purchase of a large shelf, at the expense of some labour before each firing.

Mix (by weight)The mix is largely sand with powders to coat the sand particles to reduce the amount of sticking to glass. The mix ranges from 75% sand 25% alumina hydrate, up to 67% sand, 33% alumina. The proportions can be adjusted by experience.

Some kiln formers include plaster or china clay (kaolin) in various proportions so the whole mix can range from 70% sand, 25% alumina, 5% plaster/kaolin up to 60% sand, 20% each alumina and plaster/kaolin. Some have found that the plaster started to scum up the glass after a number of firings, and this can happen with china clay too.

UseThe use of sand as the bed of the kiln requires screeding of the sand before each firing. It is possible to smooth the sand with a plaster’s float. This presses the sand down and allows a fine film of powder to coat the surface. A more certain way of avoiding the sand sticking to or texturing the glass is to lay fibre paper over the sand.

You should be aware that a sand bed requires a little different cooling than glass on a suspended shelf does. Effectively you are cooling the glass on the bed of the kiln. Thus, you should use annealing and cooling schedules for one or two thicknesses more than is actually being fired to be really safe.

Sand formingIf you are using the sand for mild shaping, sprinkle alumina hydrate over formed sand to reduce sand particle take up and textures onto the glass.

Renew sand regularly if you are using powders on the sand. An annual renewal using half the old sand mix and the rest new will be sufficient in most cases. The effect of too much powder is to promote large bubbles as air cannot move through the sand with the same ease as when there is less powder. An easy way to tell if you have too much powder is that the mix flows ahead as you screed it.

Revised 22/6/19

Formers

This post is not about the materials that go into the making of glass, but about ways of forming glass once melted or dripped into a space.

Formers are a bit different from moulds.  They are more like the formers used in concrete structures – they are there to resist the movement of the contained materials and give the form or shape desired rather than a natural flow.

These formers can be of anything that can resist the firing temperatures of the process.  Some of the materials are stainless steel, ceramics, fibre board and paper, vermiculite, kiln brick, and I am sure there are others.

Refractory Fibre

Most of these require a separator between themselves and the glass.  The ones which do not are untreated refractory fibre board and fibre paper. 

Most paper is not sufficiently strong to stand on its own. Instead it is used flat and the shape cut out of it.  It can be made in several layers and pinned together to achieve the height desired.  It should be lined in the interior with a thin fibre paper to avoid seeing the layers of the former in the edge of the glass.

For thicker work, fibre board can be used with the shape or form cut from it. Alternatively, it can be used on its side backed up by kiln brick or other material to resist movement. More information on methods and safety are here. 

If hardened, refractory board and paper will need separators between glass and former, just as most other materials will.

Sometimes the fibre board and fibre paper are not heavy enough to resist the flow of the glass.  You can use weights to help resist the movement.  At other times, the glass flows under the fibre and then you need something heavier.  Fortunately, there are a number of refractory materials that can be used.

Other common formers

Vermiculite board is another refractory material that can be cut and shaped much like fibre board.  The vermiculite needs to be covered with kiln wash where it might come into contact with glass or be lined with fibre paper or another separator.

Calcium silicate board can be used in much the same way.  It also needs a separator but does not stand up to such high temperatures as vermiculite.

Ceramics, especially in the form of cut up kiln shelves can be used as straight formers.  They have the advantage, over refractory fibre paper and boards, vermiculite and calcium silicate, of being heavy.  They can resist the movement of thick glass. They need to have a separator and usually a 3mm fibre paper, cut 3mm shorter than the final thickness of the piece, will provide the cushion in the movement that the glass needs.

Kiln brick is an often forgotten former.  The bricks can be cut and formed in many ways, even if not so freely as fibre board and paper.  The bricks do need fibre paper separators to keep the glass from getting into the pores of the brick.

Stainless steel is a common former too.  These are usually formed into an already determined shape and so are not so adaptable as many of the other formers.  Steel contracts much more than glass and needs a cushion of fibre paper, usually 3mm thick to avoid sticking to the glass.

More information on most of these formers can be found here.

Batt Wash Sticking to the Glass

The main reasons that kiln wash sticks to glass are:

1. Firing at too high a temperature. The higher the temperature, the more likely the kiln wash will stick to the glass.

2. Firing with opalescent glass against the shelf. Kiln wash sticks to opalescent glasses more easily than to transparent glass.

3. Re-using kiln washed shelves that have been to fusing temperatures already.

4. Using kiln wash with high amounts of china clay makes for more sticking. Thus some brands stick more frequently than others.

Firing at too high a temperature is probably the worse culprit. The second is using opalescent directly on the kiln shelf.


Strategies to avoid this sticking are:

1. Fire at the lowest temperature you can to get the result you want. This often requires slow rates of advance and extended soaks at the working temperature

2. Use Bullseye kiln wash. It is among the best.

3. Have a transparent glass as the bottom layer.

4. Use iridised glass, with the iridised side down to the shelf, as the iridisation acts as a separator. Do not do this with Thinfire, as it can lead to large cavities in the glass.  Fire onto kiln wash.

There are ways to get the kiln wash off but it's easier to avoid it. Using an iridised sheet on the bottom is probably the most effective prevention.  

Multiple firings of kiln wash

Pot Melt Formers

There are several suppliers of stainless steel and ceramic formers for pot melts.  They are not always necessary.

If you only want a circle, you do not need a former at all.  The shelf must be kiln washed and level.  The glass will pool in a circular manner ranging in thickness – thickest at the centre and 6-7mm at the edge. The variation in thickness depends on the time the glass is kept at the working temperature after the pot has emptied.

If you are wanting a thicker melt, you do need a dam of some sort.  You can purchase what you want, or you can make some from the materials you have at hand.

You can make a rectangle or square melt from existing straight dams.  You need to make sure the dams are kiln washed and lined with 3mm fibre paper.  You do not need to cut the dams to a predetermined length.  Instead, you can arrange them so that one end of the dam starts at the edge of your rectangle.  The next dam is butted at right angles to the first at the length wanted.  The other pieces are fitted similarly, until the last one passes the end of the first, so that they are butted together.  Then line with the fibre paper.  If you feel the dams are too light, you can back them up with bricks to prevent movement.

Using fibre paper, fibre board, or vermiculite board you can make any shape of melt that you can cut out of these materials.  If you don’t have refractory board, you can make your former out of layers of 3mm fibre paper.  It is possible to make a template for cutting of the multiple layers.  Cut your shape from the required number of layers of fibre to be as thick as your pot melt will become, according to your calculations.  Pin these layers together with stainless steel pins to be sure they do not move or float with the glass.  If you like, you can weight the layers of fibre paper with kiln furniture.

If you have refractory board – fibre or vermiculite – you can cut the required shape from them.  If you do not harden the fibre board, you do not need any further separator.  But you can line the shape with a thin fibre paper to ease the release and refine the edge.  Vermiculite always needs a separator, as it sticks to glass.  You should line the vermiculite board to get an easy release from the glass.

Using refractory materials releases you from the restrictions of commercially available forms and allows your imagination to take over.  It may not be cheaper than the bought ones, but will have the greater feeling of achievement.  In addition, you can develop all sorts of forms and depths not thought of by the commercial suppliers.

Channels in Jewellery Items

The principle in forming channels in fused glass is to keep the space open with something that will survive the firing and can be easily removed.

You can use kiln washed wire, mandrels, or tooth picks which you can pull out after cooling. These tend to leave a residue of the kiln wash behind. So this is best used on opaque items.

You can use rolled or cut fibre paper, which can be washed out after cooling, leaving a clean hole. This is works well on transparent items.

Both these methods tend to leave bumps over the channel. So you can make a three layer piece. Cut the middle layer short enough to allow the element to keep the hole open (toothpick, cut piece of fibre paper, wire etc.) to be placed with enough overlap of the top layer to catch the bottom layer. In this kind of setup you need to make the top layer a bit longer than the bottom layer. Make sure you are generous in the length of the "hole keeper" so if the glass (now possibly 9mm) does expand you do not trap the material inside.

Of course on a three layer set up like this you could use thin glass which would give you about 6mm of thickness thus eliminating the spread due to volume. In this case you would need to use fibre paper or wire that is about 1.5mm high/thick. It is probably best to have a thin piece of glass on each side of the “hole keeper” to ensure the glass does not retreat due to lack of volume.

You can experiment with a layer of standard and two of thin in various combinations to find the one you like best.

Fibre board moulds

A publication on moulds from fibre boards is available from Stained Glass Supplies. This gives much more detail than this note can.  However, the basics are outlined here.

Commonly available refractory boards are:

·         Calcium silicate

·         Standard fibre boards

·         Armstrong ceiling tiles

They can be used bare (except Armstrong ceiling tiles) or hardened.

A question that will arise is whether to harden or not.  This depends on the durability you require.  A board that is not hardened does not require kiln wash when fired.  However, as it is soft it is easy to break.  A hardened fibre board mould always requires kiln wash or another separator.  It does become durable and almost rings when tapped once it is hardened and cured.  If the shape needs to be preserved for further use, hardening is advisable.

Working methods

Usually hand tools are all that are required to get the results required.

Safety

Do any work on refractory boards outdoors if possible, and with a respirator.  If you must do it indoors, have good ventilation, wear a respirator, and clean up with damp sponges or other absorbent material to avoid putting the dust back into the air.

Do you need to pre-fire fibre moulds?

Moulds that are small or thin do not erequire firing before using.  Thick and large fibre moulds do need to have the binders burned out before use to avoid carbon marks on the glass.

Thinfire as a Separator on Moulds

"I was told that it was possible to put a piece of thinfire paper under a circular piece of glass that is to be draped over a mould....  Has anyone done this or heard of doing it?"

Yes this can be done. Some caveats are in order though.

It is important to put a separator on the mould -normally kiln wash - before using it. Once coated, it will not need to be re-coated unless the surface is damaged, scratched, etc., for a very long time. If the kiln wash seems to be rough you can smooth it in various ways as noted in this tip.  The advantage of kiln wash is that it does not cost much and lasts a long time. The thinfire or similar is a one-time-use product.

The binder in the thnifire burns away during the heat up and allows the now unbound separator to drift down to the mould before the glass begins to conform to the mould. In that way it is very similar to a fine dusting of kiln wash powder over the mould surface before firing.

I don't see the point of using Thinfire or similar during slumps (although I can see that there are occasions where this method would be useful). For drapes, placing a bit of thinfire over the mould - especially if it is metal – is an additional precaution.

My view is that you have to kiln wash the mould anyway. KIln wash is cheap and long lasting while thinfire needs to be replaced after each firing.

Lining Dams

Dams should normally be lined with Thinfire and fibre paper to get the best release. If you are using fibre board that has not been hardened, you do not have to line, but you will get smoother edges if you do.

As described by Helios

The lining papers should be about 3mm shorter than the expected final thickness of the finished panel. I find that 3mm paper against the dam provides the required standoff between the dam material and the glass. The lining of the fibre paper with Thinfire provides a smoother surface than just the fibre paper. Both of these liners should be the same height – 3mm less than the final height of the finished piece.

To calculate the expected final height you need to do a few calculations in the metric system.  Weigh the glass in grams.  Divide by specific gravity (2.5) to get the number of cubic centimeters.  Divide the cc by the area enclosed by the dams in square centimeters. This will give the fraction or multiple of centimeters thick the glass is predicted to be.  

Example:
The weight of glass = 500 gms
The specific gravity = 2.5
The area is 10cm by 10 cm = 100 square cm.

Divide 500gms (the weight) by 2.5 (the specific gravity) = 200 cubic centimeters.  Divide 200 (the volume in cc) by 100 (the area) = 2 cm thick final piece for the amount of glass put into the pot.

This indicates the fibre paper should be 1.7cm high to allow enough space for the bullnose edge to form.